• 专利标题:   Preparation of Prussian blue nanocrystalline graphene composite material used for preparing supercapacitor, includes mixing hydrochloric acid and aniline into aqueous solution, and ultrasonically dispersing graphene oxide in solution.
  • 专利号:   CN105017527-A
  • 发明人:   CHU H, QIU S, SUN L, XU F, WANG Q, XIANG C, ZOU Y
  • 专利权人:   UNIV GUILIN ELECTRONIC TECHNOLOGY
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01C003/12, C08G073/02, C08K003/04, C08K003/28, H01G011/30, H01G011/36
  • 专利详细信息:   CN105017527-A 04 Nov 2015 C08G-073/02 201617 Pages: 7 English
  • 申请详细信息:   CN105017527-A CN10385686 05 Jul 2015
  • 优先权号:   CN10385686

▎ 摘  要

NOVELTY - Preparation of Prussian blue nanocrystalline graphene composite material comprises mixing 0.1-1 mol hydrochloric acid (HCl) and 0.1-1 mol aniline into 50 ml aqueous solution; ultrasonically dispersing graphene oxide in solution obtained in first step to obtain solution-A; mixing 0.001-0.1 mol ferric nitrate, potassium ferricyanide, and HCl into 50 ml aqueous solution to obtain solution-B; slowly adding solution-A to solution-B, and magnetically stirring; standing for 2 hours, filtering, washing and drying. USE - Method for preparing Prussian blue nanocrystalline graphene composite material used for preparing supercapacitor (claimed). ADVANTAGE - The product has good conductivity. The method is simple, and has low manufacturing cost. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of supercapacitor comprising ultrasonically dispersing 5-20 mg composite material in 1-2 ml N,N-dimethylformamide solution, adding 50 mu L 5% Nafion (RTM: perfluoro-sulfonic acid polymer) solution, dropping 10-20 mu L nanocomposite suspension on surface of glass carbon electrode, and drying under infrared lamp; preparing into supercapacitor electrode, electrochemically testing charge-discharge performance using 0.1 mol/L potassium chloride solution having a pH of 5.