• 专利标题:   Preparing giant magneto-impedance effect graphene/nanocrystalline composite material comprises e.g. placing iron-based amorphous strip in tubular furnace, annealing to obtain iron-based nanocrystalline strips, and placing in quartz boat.
  • 专利号:   CN112813407-A
  • 发明人:   SONG Y, ZHAO Z, SUN Z, CHEN Y
  • 专利权人:   UNIV EAST CHINA NORMAL
  • 国际专利分类:   C21D001/26, C21D001/74, C21D009/52, C23C016/02, C23C016/26, C23C016/52
  • 专利详细信息:   CN112813407-A 18 May 2021 C23C-016/26 202152 Pages: 8 Chinese
  • 申请详细信息:   CN112813407-A CN11639975 31 Dec 2020
  • 优先权号:   CN11639975

▎ 摘  要

NOVELTY - Preparing giant magneto-impedance effect graphene/nanocrystalline composite material comprises e.g. (1) taking one iron-based amorphous iron-copper-niobium-silicon-boron (Fe73.5 Cu1 Nb3 SiB9.5) strip; (2) placing the iron-based amorphous strip obtained in the step (1) in a tubular furnace, setting vacuum degree to 0.1-5 pa, raising temperature to 540 degrees C, introducing hydrogen gas of 5-50 sccm, and annealing for 15-30 minutes to obtain iron-based nanocrystalline strips; (3) placing the iron-based nanocrystalline strip obtained in step (2) in quartz boat, and placing it in the constant temperature growth area in the middle of the tubular furnace; and (4) taking 1-10 g polymethyl methacrylate (PMMA) and placing it in quartz boat, placing it in the temperature range of 120-180 degrees C at the air inlet of tubular furnace. USE - The method is useful for preparing giant magneto-impedance effect graphene/nanocrystalline composite material. ADVANTAGE - The method: improves compatibility of directly growing graphene on strip, so that soft magnetic properties of nanocrystalline strip can be maintained. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for giant magneto-impedance effect graphene/nanocrystalline composite material is prepared by above mentioned method.