• 专利标题:   Preparing high heat-conducting graphene film to communication, electronic, aerospace, and medical treatment, involves mechanically crushing artificial graphite film to obtain artificial graphite powder, mixing graphite oxide in solvent containing ammonia water, and stirring.
  • 专利号:   CN114314573-A, CN114314573-B
  • 发明人:   SUN D, LIN L, FANG C, HONG J, HUANG W, LIN J
  • 专利权人:   XIAMEN KNANO GRAPHENE TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/19, C01B032/194
  • 专利详细信息:   CN114314573-A 12 Apr 2022 C01B-032/19 202242 Chinese
  • 申请详细信息:   CN114314573-A CN11682845 31 Dec 2021
  • 优先权号:   CN11682845

▎ 摘  要

NOVELTY - Preparing high heat-conducting graphene film involves mechanically crushing the artificial graphite film, until the fineness is less than or equal to 100 meshes to obtain artificial graphite powder. The graphite oxide is mixed in the solvent containing ammonia water, stirred uniformly and then peeled to obtain oxidized graphene, mixed the artificial graphite powder, mixed the oxidized graphene slurry with the peeling agent, stirred uniformly, then performed secondary peeling to obtain mixed slurry, the mass ratio of the oxidized graphene pulp and the artificial graphite powder is 1:0.005-1:0.5, defoamed the mixed slurry, coated on the base material, formed a thickness of 1-10 mm of graphene film, dry processed, peeled off to obtain graphene film crude product, where the temperature of drying is 65-140degrees Celsius. USE - Method for preparing high heat-conducting graphene film used to communication, electronic, aerospace, and medical treatment. ADVANTAGE - The method has high heat conductivity, effectively improves the radiating performance of the material and reduces the cost. DETAILED DESCRIPTION - Preparing high heat-conducting graphene film involves mechanically crushing the artificial graphite film, until the fineness is less than or equal to 100 meshes to obtain artificial graphite powder. The graphite oxide is mixed in the solvent containing ammonia water, stirred uniformly and then peeled to obtain oxidized graphene, mixed the artificial graphite powder, mixed the oxidized graphene slurry with the peeling agent, stirred uniformly, then performed secondary peeling to obtain mixed slurry, the mass ratio of the oxidized graphene pulp and the artificial graphite powder is 1:0.005-1:0.5, defoamed the mixed slurry, coated on the base material, formed a thickness of 1-10 mm of graphene film, dry processed, peeled off to obtain graphene film crude product, where the temperature of drying is 65-140degrees Celsius. The graphene film crude product is placed in inert atmosphere, heated to the first temperature, carbonized for a certain time, placed the product in an inert atmosphere, heated to a second temperature, graphitized for a certain time to obtain the graphene film, laminated and rolled the graphene to reach the preset thickness to obtain product, where the density of the graphene film is greater than or equal to 1.8g/ml.