• 专利标题:   Preparation of graphene composite silicon carbonitride precursor ceramic by mixing polysilazane and graphene, heating, pulverizing in vibrating ball mill, sieving, press-forming, cold isostatic pressing, and heating.
  • 专利号:   CN108164268-A
  • 发明人:   GONG H, FENG Y, ZHANG Y, GUO X, LIU Y, LIN X, MAO J
  • 专利权人:   UNIV SHANDONG
  • 国际专利分类:   C04B035/584
  • 专利详细信息:   CN108164268-A 15 Jun 2018 C04B-035/584 201851 Pages: 9 Chinese
  • 申请详细信息:   CN108164268-A CN11483578 29 Dec 2017
  • 优先权号:   CN11483578

▎ 摘  要

NOVELTY - Preparation of graphene composite silicon carbonitride precursor ceramic by precursor method comprises mixing polysilazane and graphene uniformly at mass ratio of 60-95:5-40 under nitrogen atmosphere to obtain mixed solution; heating from room temperature to 300-800 degrees C at heating rate of 3-5 degrees C/minute for 1-8 hours; pulverizing in vibrating ball mill and passing through 100-200 mesh sieve; press-forming under 5-15 MPa pressure, cold isostatic pressing at 150-250 MPa, and holding pressure for 200-400 seconds to obtain green body; and heat-treating under nitrogen gas protection at 1000-1300 degrees C for 2-6 hours. USE - Method for preparing graphene composite silicon carbonitride precursor ceramic. ADVANTAGE - The method increases relative complex dielectric constant, increases loss factor, and improves reflection loss of material.