• 专利标题:   Preparation of porous graphene-coated lithium-vanadium phosphate involves mixing e.g. citric acid and water, adding vanadium pentoxide powder, stirring, adding lithium carbonate, stirring, adding porous graphene, and heat-treating.
  • 专利号:   CN111883747-A
  • 发明人:   XU J, LU H, ZHAO S, XIAO F, LEI Y, HUANG C
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M010/54, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN111883747-A 03 Nov 2020 H01M-004/36 202097 Pages: 12 Chinese
  • 申请详细信息:   CN111883747-A CN10590457 24 Jun 2020
  • 优先权号:   CN10590457

▎ 摘  要

NOVELTY - Preparation of porous graphene-coated lithium-vanadium phosphate involves adding citric acid and ammonium hydrogen phosphate to water, uniformly stirring, obtaining a colorless and transparent solution, adding vanadium pentoxide powder to the colorless and transparent solution, uniformly stirring, obtaining an orange solution, adding lithium carbonate to the orange solution, heating in a water bath under stirring, obtaining a dark green solution, adding porous graphene prepared by recycling graphite from waste power batteries to the dark green solution, stirring, heat-treating obtained dark black solution, drying obtained sol, grinding, adding obtained dark black powder to a reactor, introducing a mixed gas of argon and hydrogen, heating, cooling to room temperature, pressing obtained powder into a sheet material, placing the sheet material in the reactor, introducing mixed gas of argon and hydrogen, heating, then cooling to room temperature, and grinding into powder. USE - Preparation of porous graphene-coated lithium-vanadium phosphate. ADVANTAGE - The method enables economical preparation of porous graphene-coated lithium-vanadium phosphate with high yield. The porous graphene provides more active sites to lithium-vanadium phosphate, and the pores on porous graphene have favorable transmission of electrons and electrolyte.