▎ 摘　　要

NOVELTY - Performing PI film environment-friendly production technique involves adding diacyl chloride with alkali A catalyst, eight ammonia B for reaction condensation, under the continuous catalytic chemical reaction of high temperature, condensation reaction to phthalimide, under the DAXNER reactor, continuous continuous reaction. The stable temperature control pressure control reactor of DAXNER reactor for continuity. The continuous automatic quantitative benzene anhydride process is finished by the automatic supply system of DAXNERreactor. The whole process flow is automatically controlled by DAXNER reactor, automatic execution,continuous, online, continuously automatic feeding,automatic temperature adjusting, continuously reacting, automatic high precision system, automatic pressure adjusting system, continuously separating, the proper stage is continuously extracted, automatic relay continuous safety reaction and amination reaction to obtain N5-methyl-5-NO2-phthalimide. USE - Method for performing PI film environment-friendly production technique in electronic skin, transparent graphite graphene conductive film, soluble lithium battery. ADVANTAGE - The method ensures the reliability, and the stability of the supply, the coal rotating clean fuel methanol. DETAILED DESCRIPTION - Performing PI film environment-friendly production technique involves adding diacyl chloride with alkali A catalyst, eight ammonia B for reaction condensation, under the continuous catalytic chemical reaction of high temperature, condensation reaction to phthalimide, under the DAXNER reactor, continuous reaction. The stable temperature control pressure control reactor of DAXNER reactor for continuity. The continuous automatic quantitative benzene anhydride process is finished by the automatic supply system of DAXNERreactor. The whole process flow is automatically controlled by DAXNER reactor, automatic execution, continuous, online, continuously automatic feeding, automatic temperature adjusting, continuously reacting, automatic high precision system, automatic pressure adjusting system, continuously separating, the proper stage is continuously extracted, automatic relay continuous safety reaction and amination reaction to obtain N5-methyl-5-NO2-phthalimide. The bis - (N5-methyl-5-NO2 phthalimide) is prepared by using10-dendrobium N5-methyl-5-NO2-phthalimide, the Bipolar non-proton transfer organic solvent is solvent,the nitrite-base-carbonic-base of metal of 50 hopper is composite high-efficiency catalytic reaction agent, under the high pressure of 50 MPa, heating and refluxing for 1-2 hours, continuous online continuous reaction, heating high pressure, the DAXNER special development device, the needed F solvent, to DAXNER filtered after quantitative adding water and F solvent stirred and filtered, the middle process does not generate by-product, no wastewater, generate waste gas, waste material, filter, circulate water washing fine filter after flaking, after the high-efficient hydrolysis system, deeply hydrolyzing,entering the next system process, through the acidification device, automatic acidification, making the material fully reach the acidification effect, automatic acid value control technology, automatically entering the next set of process technology processing device after meeting the reasonable acidification value. The pre-processing process enter the green circulating decoloring system device, the raw material automatic recycling treatment, active carbon harmless treatment and recycling, automatic monitoring decoloring cost device, when the decoloring is finished, and can realize automatic monitoring detection, detect the qualified portion, automatically entering the next process device, forming anhydride, the whole process is automatic, sealing operation. The prepared anhydride and ODA, NMP, PMDA, DMAC is decolorized, prepared, and produce low carbon type benzene type polyimide resin, use solution circulation online polycondensation to synthesize precursor raw material high purity polyamic acid, after entering the next process, introducing DAXNER dehydration cyclizing circulating green environment-friendly device to prepare polyimide resin film, specifically as follows 8 hoppers of pyromellitic dianhydride and precision equimolar ratio of 8 hopper diamino diphenyl ether in the polar solvent dimethylacetamide by DAXNER high-pressure reactor to react, synthesizing the precursor as 50 % purity of polyamic acid, entering into the next process DAXNER connecting-loop online holding three-linked high pressure reactor, keeping the reaction to reach 5 high purity polyamic acid, then through DAXNERdehydration cyclizing circulating green environment-friendly device closed loop imidization to prepare the purity polyimide resins.