• 专利标题:   Method for preparing anode of solid oxide fuel battery by two-dimensional material assisted impregnation, involves adding graphite oxide to deionized water, adding ammonia solution and loading graphene oxide solution with nickel hydroxide.
  • 专利号:   CN108550866-A
  • 发明人:   TIAN Y, NIE Z, GUO X, ZHAI A, LIU C
  • 专利权人:   UNIV TAIYUAN TECHNOLOGY
  • 国际专利分类:   H01M004/88
  • 专利详细信息:   CN108550866-A 18 Sep 2018 H01M-004/88 201869 Pages: 13 Chinese
  • 申请详细信息:   CN108550866-A CN10408506 02 May 2018
  • 优先权号:   CN10408506

▎ 摘  要

NOVELTY - A solid oxide fuel anode battery preparing method involves adding graphite oxide to deionized water, magnetic stirring and ultrasonic dispersion at room temperature for 0.5-24 hour and configuring into a graphene oxide solution, weighing nickel nitrate into deionized water to obtain a nickel nitrate solution at a concentration of 5-50 mmol/L, adding a concentration of 25-28% ammonia solution until completely dissolved, adding the mixed solution in a graphene oxide solution, magnetically stirring or sonicating, loading graphene oxide solution with nickel hydroxide is introducing into the porous anode support body by dipping and after lyophilization, the temperature is raised to 300-500 degrees C for 0.5-4 hour under the protection of an argon atmosphere to obtain a supported reduction oxidation, impregnating anode with graphene-supported nickel oxide in a hydrogen atmosphere at 600-800 degrees C for 1-4 hours to reduce nickel oxide to nickel to obtain the finished product. USE - Method for preparing anode of solid oxide fuel battery by two-dimensional material assisted impregnation. ADVANTAGE - The method enables preparing anode of solid oxide fuel battery with enhanced stability and conductivity and catalytic performance of the anode.