• 专利标题:   Preparing graphene useful e.g. in battery fields, electronics and energy storage materials, comprises performing intercalation oxidation of graphite to obtain graphite oxide acidic dispersion liquid and reducing with amino phenol compound.
  • 专利号:   CN103373726-A, CN103373726-B
  • 发明人:   LIU G, SUN P, WU G, WU Z
  • 专利权人:   TORAY ADVANCED MATERIALS RES LAB, TORAY ADVANCED MATERIALS RES LAB
  • 国际专利分类:   C01B031/04, C01B032/19
  • 专利详细信息:   CN103373726-A 30 Oct 2013 C01B-031/04 201413 Pages: 8 Chinese
  • 申请详细信息:   CN103373726-A CN10130981 19 Apr 2012
  • 优先权号:   CN10130981

▎ 摘  要

NOVELTY - Preparing graphene comprises carrying out intercalation oxidation of graphite to obtain graphite oxide acidic dispersion liquid, then adding reducing agent to the acidic dispersion to give graphene, where the reducing agent is substituted amino phenol or its salt (I). USE - Graphene useful in battery fields, composites, electronics and energy storage materials. ADVANTAGE - The method: does not require washing of dispersion liquid neutral or slightly acidic, utilizes less time and improves production efficiency. DETAILED DESCRIPTION - Preparing graphene comprises carrying out intercalation oxidation of graphite to obtain graphite oxide acidic dispersion liquid, then adding reducing agent to the acidic dispersion to give graphene, where the reducing agent is substituted amino phenol compound of formula (I) or its salts. R1, R2 = H, 1-99C alkyl, benzyl, 1-99C alkenyl, phenyl, 1-99C cycloalkyl, 2-99C cycloalkenyl or 1-99C heteroaryl.