• 专利标题:   Preparing graphene comprises adding mixture of graphite oxide and water in aqueous ammonia, stirring the mixture, centrifuging the graphite oxide in centrifuge, pouring the supernatant, and mixing obtained product with hydrazine hydrate.
  • 专利号:   CN103408003-A, CN103408003-B
  • 发明人:   WANG L, ZHAO W, QI T, QU J, WANG Y, HAN P
  • 专利权人:   INST PROCESS ENG CHINESE ACAD SCI
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103408003-A 27 Nov 2013 C01B-031/04 201414 Pages: 6 Chinese
  • 申请详细信息:   CN103408003-A CN10325054 30 Jul 2013
  • 优先权号:   CN10139039, CN10325054

▎ 摘  要

NOVELTY - Preparing graphene comprises adding mixture of graphite oxide and water in aqueous ammonia, stirring the mixture for 10-30 minutes, adjusting pH value of the solution to 7-8 degrees C and then standing for 5-10 minutes, centrifuging the graphite oxide in a centrifuge for 5-65 minutes, pouring the supernatant to obtain neutral graphite oxide deposition, mixing obtained product with hydrazine hydrate according to volume ratio of 1:5-5:1, ultrasonically dispersing in the solution at 150-250 degrees C for 10-60 hours, and filtering the dispersed solution and then washing by water and drying. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method simply and economically prepares the graphene with high yield.