• 专利标题:   Manufacturing graphene, by adding graphite powder and water to reactor, stirring and heating sealed reactor, cooling mixture, performing centrifugal separation and subjecting graphene dispersion to high speed centrifugal separation.
  • 专利号:   CN103771402-A
  • 发明人:   DONG H, LIU X, LIU Y, LEI B, ZHANG H, XIAO Y, ZHENG M
  • 专利权人:   UNIV SOUTH CHINA AGRIC
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103771402-A 07 May 2014 C01B-031/04 201444 Pages: 11 Chinese
  • 申请详细信息:   CN103771402-A CN10747304 30 Dec 2013
  • 优先权号:   CN10747304

▎ 摘  要

NOVELTY - Manufacturing graphene, by adding graphite powder and water to reactor, sealing the reactor, stirring, heating the reactor to reaction temperature, performing constant stirring process continuously, cooling reaction mixture, taking out mixed reacted solution from the reactor, subjecting solution to centrifugal separation to obtain pellet at lower portion and liquid supernatant at upper portion, and subjecting obtained graphene dispersion to high speed centrifugal separation to obtain solid graphene. USE - The method is useful for manufacturing solid graphene (claimed). ADVANTAGE - The method utilizes water as solvent to overcome high boiling point, toxicity, difficulty associated with its removal and solubility of organic solvents, which does not satisfies solubility parameters of the graphene dispersion and leads to relatively lower or insufficient concentration of the graphene. The method provides high yield of the graphene with fewer defects, low oxygen content and maintained original electrical properties of the graphite. DETAILED DESCRIPTION - Method for manufacturing graphene, involves (a) adding graphite powder and water to reactor, (b) sealing the reactor, stirring, heating the reactor to reaction temperature and performing constant stirring process continuously after completion of the reaction, (c) cooling reaction mixture, taking out mixed reacted solution from the reactor, subjecting the solution to centrifugal separation to obtain pellet at lower portion and liquid supernatant at upper portion, where solid substances present at the lower portions are un-reacted solid graphite powder and the liquid supernatant is graphene dispersion, and (d) subjecting the graphene dispersion to high speed centrifugal separation to obtain solid graphene.