• 专利标题:   Preparing graphene antimony nanotube cathode material for sodium ion battery, involves making certain mole amount of sodium sulfide and dissolving in glycol to obtain first precursor solution and making certain mole of antimony chloride.
  • 专利号:   CN108400298-A
  • 发明人:   SUO G, BI Y, YANG Y, FENG L, HOU X, LI D, CHEN H, AO D, ZHAN S, ZUO Y, ZHANG Z, GONG Y, ZHU J
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   H01M010/054, H01M004/36, H01M004/38, H01M004/583
  • 专利详细信息:   CN108400298-A 14 Aug 2018 H01M-004/36 201863 Pages: 10 Chinese
  • 申请详细信息:   CN108400298-A CN10128489 08 Feb 2018
  • 优先权号:   CN10128489

▎ 摘  要

NOVELTY - Preparing graphene antimony nanotube cathode material involves making certain mole amount of sodium sulfide and dissolving in glycol to obtain first precursor solution, making certain mole of antimony chloride and dissolving in glycol to obtain second precursor solution, adding first precursor solution with stirring in second precursor solution to obtain third solution, where molar ratio of sodium sulfide and antimony is 1-3:3, dispersing certain concentration of graphene dispersion into third solution, and transferring to polytetrafluoroethylene liner at high pressure kettle at 120 degrees C and keeping for 3 hours to obtain synthesis product, separating solvent thermal synthesis product through 10000 revolutions/minute, washing with de-ionized water and ethanol, drying at 85 degrees C to obtain fifth product, reacting obtained product for 12 hours and mixing with hydrogen and argon gas atmosphere, annealing at 350 degrees C for 12 hours to obtain graphene antimony nano-composite. USE - Method for preparing graphene antimony nanotube cathode material for sodium ion battery. ADVANTAGE - The method enables to prepare graphene antimony nanotube cathode material has high recycle ratio capacity, coulombic efficiency and stable cycle performance.