• 专利标题:   Reduction of combustion slagging rate of corn straw biomass pellet fuel includes weighing graphene, adding dimethyl formamide solvent, mixing, performing ultrasonic dispersion, ball milling, washing with ethanol, drying, heating and cooling.
  • 专利号:   CN108949285-A
  • 发明人:   YAN X
  • 专利权人:   HEFEI JINGGU AGRIC TECHNOLOGY DEV CO LTD
  • 国际专利分类:   C10L009/10, C10L005/44, C04B038/02, C04B035/16, C04B035/622
  • 专利详细信息:   CN108949285-A 07 Dec 2018 C10L-009/10 201914 Pages: 7 Chinese
  • 申请详细信息:   CN108949285-A CN10787515 18 Jul 2018
  • 优先权号:   CN10787515

▎ 摘  要

NOVELTY - Reduction of combustion slagging rate of corn straw biomass pellet fuel comprises weighing 5.5-6 g graphene, adding 150-160 ml dimethyl formamide solvent, mixing, performing ultrasonic dispersion for 8-10 minutes, adding 0.5-0.8 g sodium dodecyl sulfate, ball milling for 7-8 hours, standing for layering, performing high-speed centrifugation for 50-60 seconds to obtain suspension liquid, performing reduced pressure distillation to remove solvent, washing with ethanol for 2-3 times, drying in 80-90 degrees C oven to obtain purified graphene, mixing purified graphene, alumina powder and polyvinyl alcohol, adding 2.7-3 times deionized water, mixing for 1-2 hours, performing ultrasonic treatment for 1.5-2 hours, heating, mixing, evaporating, precipitating solid product at 50-60 degrees C in vacuum drying oven, drying to obtain graphene composite material, grinding dried loess and bentonite, sieving, mixing, drying, pre-heating, firing and cooling. USE - Method of reducing combustion slagging rate of corn straw biomass pellet fuel. ADVANTAGE - The method improves ash melting point of corn straw granule fuel, has maximum utilization of resources and protects the environment. DETAILED DESCRIPTION - Reduction of combustion slagging rate of corn straw biomass pellet fuel comprises weighing 5.5-6 g graphene, adding 150-160 ml dimethyl formamide solvent, mixing at 1800-2000 revolutions per minute (rpm) for 20-30 minutes, performing ultrasonic dispersion for 8-10 minutes, adding 0.5-0.8 g sodium dodecyl sulfate, ball milling for 7-8 hours, standing for layering, performing high-speed centrifugation for 50-60 seconds to obtain suspension liquid, performing reduced pressure distillation to remove solvent, washing with ethanol for 2-3 times, drying in 80-90 degrees C oven to obtain purified graphene, mixing purified graphene, alumina powder and polyvinyl alcohol at 0.2-0.3:2.5-3:4-5, adding 2.7-3 times deionized water, mixing for 1-2 hours, performing ultrasonic treatment for 1.5-2 hours, heating, mixing, evaporating to remove moisture, precipitating solid product at 50-60 degrees C in vacuum drying oven, drying for 8-10 hours to obtain graphene composite material, grinding dried loess and bentonite at 2-3:1-2, sieving powder to 0.5-0.6 mm square mesh, mixing, drying at 100-110 degrees C for 2-3 hours, pre-heating in high-temperature furnace, firing for 24-28 minutes at 1280-1300 degrees C and cooling to 25-30 degrees C.