• 专利标题:   Preparing nanosheet graphene powder involves mixing methyl methacrylate, 2-(dimethylamino)ethyl methacrylate, azo-bis-isobutyrynitrile, dibenzoyl peroxide and industrial grade methyl methacrylate.
  • 专利号:   CN105315593-A, CN105315593-B
  • 发明人:   LIU X, ZHOU Q
  • 专利权人:   UNIV QIQIHAR
  • 国际专利分类:   C08F220/14, C08F220/34, C08K003/04, C08L033/12
  • 专利详细信息:   CN105315593-A 10 Feb 2016 C08L-033/12 201632 Pages: 5 English
  • 申请详细信息:   CN105315593-A CN10879367 05 Dec 2015
  • 优先权号:   CN10879367

▎ 摘  要

NOVELTY - Nanosheet graphene powder preparation involves mixing 0.03g methyl methacrylate, 9.5g 2-(dimethylamino)ethyl methacrylate, 0.5g azo-bis-isobutyrynitrile, 0.05g dibenzoyl peroxide and 0.006 g industrial grade methyl methacrylate. The obtained mixture is purified with decompression distillation method. The obtained mixture is ultrasonically cleaned for 2 hours. The obtained mixture is kept in a three three-necked bottle. The obtained three-necked bottle is equipped with condensation pipe, stirrer and nitrogen entrance. The obtained mixture is added with 0.05g azo-bis-isobutyrynitrile. USE - Method for preparing nanosheet graphene powder (claimed). DETAILED DESCRIPTION - Nanosheet graphene powder preparation involves mixing 0.03g methyl methacrylate, 9.5g 2-(dimethylamino)ethyl methacrylate, 0.5g azo-bis-isobutyrynitrile, 0.05g dibenzoyl peroxide and 0.006 g industrial grade methyl methacrylate. The obtained mixture is purified with decompression distillation method. The obtained mixture is ultrasonically cleaned for 2 hours. The obtained mixture is kept in a three three-necked bottle. The obtained three-necked bottle is equipped with condensation pipe, stirrer and nitrogen entrance. The obtained mixture is added with 0.05g azo-bis-isobutyrynitrile. The obtained mixture is stirred. The temperature of the mixture is raised at 80 degrees C for 1 hours. The temperature of the mixture is reduced at 50 degrees C. The obtained mixture is poured in a test-tube. The obtained test tube is kept in a water bath at 50 degrees C.