• 专利标题:   Preparing three-dimensional graphene powder material of carbon containing polymer, involves adding polymeric monomer, cross-linking agent monomer and initiator, adding pore-forming agent and dispersant, and cooling with water.
  • 专利号:   CN106986960-A
  • 发明人:   SHEN P, SUN X, TIAN Z, QIU Z
  • 专利权人:   UNIV GUANGXI
  • 国际专利分类:   C08F002/20, C08F212/10, C08F212/36, C08F220/06, C08F220/14, C08F220/28, C08F220/46, C08F222/14, C08F222/26, C08F226/06, C08F285/00, C08J009/26, C08L025/14
  • 专利详细信息:   CN106986960-A 28 Jul 2017 C08F-212/10 201764 Pages: 8 Chinese
  • 申请详细信息:   CN106986960-A CN10984848 09 Nov 2016
  • 优先权号:   CN10984848

▎ 摘  要

NOVELTY - Preparing three-dimensional graphene powder material of carbon containing polymer, involves adding 87-99wt.% of polymeric monomer, 0.5-10wt.% of cross-linking agent monomer and 0.5-3.0wt.% of initiator and stirring to obtain the monomer phase. The pore-forming agent is added and then stirred. The aqueous solution is added into the reaction kettle, and then dispersant is added. The monomer is dripped into the reaction kettle at 60-95 degrees C for 6-5 hours, and then cooled to room temperature, washed with water. USE - Method for preparing three-dimensional graphene powder material of carbon containing polymer (claimed). ADVANTAGE - The method enables to Prepare three-dimensional graphene powder material of carbon containing polymer in a simple and convenient operation. The polymer has crumbling rate of /- 98%. The obtained product is stable and has high purity. DETAILED DESCRIPTION - Preparing three-dimensional graphene powder material of carbon containing polymer, involves adding 87-99wt.% of polymeric monomer, 0.5-10wt.% of cross-linking agent monomer and 0.5-3.0wt.% of initiator and stirring to obtain the monomer phase. The pore-forming agent is added and then stirred. The aqueous solution is added into the reaction kettle, and then dispersant is added. The monomer is dripped into the reaction kettle at 60-95 degrees C for 6-5 hours, and then cooled to room temperature, washed with water, dehydrated and dried to obtain copolymer whose grain size is 0.15-1.2 mm. The extracting agent is added in the copolymer containing pore-forming agent, and then hydrolyzing agent is added to hydrolyze to obtain the resulting copolymer. The copolymer is washed by water, and dried to obtain the graphene powder three-dimensional structure material carbon-containing polymer.