• 专利标题:   Preparation of graphene masterbatch, involves grinding graphene and blowing agent, dispersing to obtain graphene-blowing agent dispersion, and spraying into spray condenser through high pressure liquid nitrogen stream.
  • 专利号:   CN107022113-A, CN107022113-B
  • 发明人:   CHEN Q, ZENG J
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD, CHENGDU NEW KELI CHEM ENG SCI TECHNIC
  • 国际专利分类:   C08K003/04, C08K009/02, C08K009/04, C08L021/00, C08L023/12
  • 专利详细信息:   CN107022113-A 08 Aug 2017 C08K-009/02 201765 Pages: 8 Chinese
  • 申请详细信息:   CN107022113-A CN10353235 18 May 2017
  • 优先权号:   CN10353235

▎ 摘  要

NOVELTY - The preparation method of graphene masterbatch involves (i) grinding graphene and blowing agent, uniformly dispersing at low temperature to obtain a graphene-blowing agent dispersion, (ii) spraying graphene-blowing agent dispersion into a spray condenser through a high pressure liquid nitrogen stream, laterally spraying high temperature melting and low-temperature condensing material into a spray condenser to form a transverse curtain, (iii) condensing transverse curtain and graphene-blowing agent dispersion into bead-like particles, and spraying into bottom of spray condenser. USE - Preparation of graphene masterbatch (claimed). ADVANTAGE - The method enables the preparation of graphene masterbatch with excellent dispersion property and agglomeration resistance. DETAILED DESCRIPTION - The preparation method of graphene masterbatch involves (i) grinding 60-70 pts. wt. graphene and 10-15 pts. wt. blowing agent, uniformly dispersing at low temperature to obtain a graphene-blowing agent dispersion, (ii) spraying graphene-blowing agent dispersion into a spray condenser in the form of a spray through a high pressure liquid nitrogen stream at the top of the spray condenser, laterally spraying high temperature melting and low-temperature condensing material in the form of a spray into a spray condenser to form a transverse curtain, (iii) rapidly condensing transverse curtain and graphene-blowing agent dispersion into bead-like particles, and spraying into bottom of spray condenser through high pressure liquid nitrogen stream.