• 专利标题:   Producing graphene film, comprises e.g. ultrasonically cleaning a metal substrate with hydrochloric acid, acetone, and deionized water to remove moisture content on surface, subjecting to high temperature annealing, and uniformly cooling.
  • 专利号:   CN106587030-A, CN106587030-B
  • 发明人:   HU B, ZHAO W
  • 专利权人:   UNIV CHONGQING, UNIV CHONGQING
  • 国际专利分类:   C01B032/186, C23C016/02, C23C016/26
  • 专利详细信息:   CN106587030-A 26 Apr 2017 C01B-032/186 201734 Pages: 8 Chinese
  • 申请详细信息:   CN106587030-A CN10018061 11 Jan 2017
  • 优先权号:   CN10018061

▎ 摘  要

NOVELTY - Producing graphene film, comprises e.g. (a) ultrasonically cleaning a metal substrate with hydrochloric acid, acetone, and deionized water for 5-10 minute to remove moisture content on the surface, and subjecting the metal substrate to high temperature annealing at 850-1050 degrees C under argon flow rate of 300-1000 sccm and hydrogen flow rate of 10-100 sccm for 10-90 minutes, (b) uniformly cooling at 200-800 degrees C under argon atmosphere with argon gas flow rate of 300-1000 sccm, and (c) lowering to predetermined reaction temperature. USE - The method is useful for producing graphene film (claimed). ADVANTAGE - The method produces graphene film with high quality and uniform layers, and is simple and economical. DETAILED DESCRIPTION - Producing graphene film, comprises (a) ultrasonically cleaning a metal substrate with hydrochloric acid, acetone, and deionized water for 5-10 minute to remove moisture content on the surface, and subjecting the metal substrate to high temperature annealing at 850-1050 degrees C under argon flow rate of 300-1000 sccm and hydrogen flow rate of 10-100 sccm for 10-90 minutes, (b) uniformly cooling at 200-800 degrees C under argon atmosphere with argon gas flow rate of 300-1000 sccm, and (c) lowering to predetermined reaction temperature, and introducing carbon gas source and argon gas to chemical vapor deposition to obtain a graphene film.