• 专利标题:   Preparation of graphene, involves mixing carbon source, carrier gas and additive, preheating, passing into plasma generator, pulverizing carbon source, adding to fluidized bed device, and separating reacted gas-solid mixture and graphene.
  • 专利号:   CN108557809-A
  • 发明人:   HONG R, GAO M, WANG W, WANG F
  • 专利权人:   UNIV FUZHOU
  • 国际专利分类:   C01B032/184, C01B003/22, C01B003/24
  • 专利详细信息:   CN108557809-A 21 Sep 2018 C01B-032/184 201873 Pages: 12 Chinese
  • 申请详细信息:   CN108557809-A CN10834000 26 Jul 2018
  • 优先权号:   CN10834000

▎ 摘  要

NOVELTY - The preparation method of graphene involves (1) mixing a carbon source, carrier gas and additive according to a certain proportion in a buffer tank, preheating by a heat exchanger, passing into a plasma generator, where the discharge voltage of the plasma generator is 360-100 kV, the current is 0.1-100 A, and the temperature is 800-6500 degrees C, and (2) pulverizing the carbon source by plasma generator, adding to a fluidized bed device to promote cracking of carbon source and nucleation and growth of graphene, separating the reacted gas-solid mixture and graphene through a cyclone separator, circulating into a buffer tank after the exhaust gas is separated by the cyclone separator, and passing into the plasma generator for recycling with the mixed gas. USE - Preparation method of graphene. ADVANTAGE - The method enables preparation of graphene which does not require harsh conditions and produce waste, and recycles portion of un-cracked carbon source.