• 专利标题:   Synthesizing graphene-coated manganese oxide nanomaterial by adding manganese oxide nanomaterial to water, adding graphene oxide to water, dripping graphene oxide solution into manganese oxide, freeze-drying, annealing powder, and heating.
  • 专利号:   CN110817967-A
  • 发明人:   FENG Q, LIN Y
  • 专利权人:   UNIV FUJIAN
  • 国际专利分类:   B82Y030/00, C01B032/184, C01G045/02, H01M010/0525, H01M010/058, H01M004/50, H01M004/62
  • 专利详细信息:   CN110817967-A 21 Feb 2020 C01G-045/02 202024 Pages: 8 Chinese
  • 申请详细信息:   CN110817967-A CN11095717 11 Nov 2019
  • 优先权号:   CN11095717

▎ 摘  要

NOVELTY - Method for synthesizing graphene-coated manganese oxide nanomaterial by microwave-assisted method, involves (a) adding manganese oxide nanomaterial to water, and uniformly dispersing by magnetic stirring and ultrasonically processing to obtain a manganese oxide solution, (b) adding graphene oxide to water, and dissolving by magnetic stirring and ultrasonically processing to obtain a graphene oxide solution, (c) slowly dripping graphene oxide solution into manganese oxide solution, and freeze-drying the mixed solution to obtain manganese oxide doped graphene oxide powder, and (d) annealing the powder in an argon gas atmosphere in a tube furnace for 1-1.2 hours to obtain a precursor, placing obtained precursor in a closed glass bottle filled with argon gas, and heating the glass bottle in a microwave oven to obtain the nanomaterial. USE - The method is useful for synthesizing graphene-coated manganese oxide nanomaterial used in lithium ion battery anode material. ADVANTAGE - The method reduces graphene through microwave instant high temperature, and effectively repairs the defects of graphene, and the prepared nanomaterial has excellent electrochemical performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for use of the graphene-coated manganese oxide nanomaterial in a lithium ion battery anode material, which is prepared by the above-mentioned method.