• 专利标题:   Preparing nickel nanoparticle-graphene-foam nickel composite material used in e.g. battery, by performing current deposition using graphene-foam nickel base material, silver-silver chloride and nickel sulfate-sulfuric acid solution.
  • 专利号:   CN107904570-A
  • 发明人:   GUO X, ZHU L, CHEN Z, LIU Y, ZHAO L, ZHANG W, LIU C, JIN K, YIN L
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   C22F001/10, C23C016/02, C23C016/26, C23F017/00, C25D003/12
  • 专利详细信息:   CN107904570-A 13 Apr 2018 C23C-016/26 201833 Pages: 4 Chinese
  • 申请详细信息:   CN107904570-A CN11084219 07 Nov 2017
  • 优先权号:   CN11084219

▎ 摘  要

NOVELTY - Preparation of nickel nanoparticle-graphene-foam nickel composite material involves heat-treating foamed nickel in quartz tube, annealing, adding methane and hydrogen to grow graphene, rapidly reducing, cooling to room temperature to obtain foam nickel material covered with graphene to form graphene-foam nickel base material and carrying out current deposition using graphene-foam nickel base material as working electrode, platinum as counter electrode, silver-silver chloride as reference electrode and nickel sulfate-sulfuric acid mixed solution as electrolyte. USE - Preparation of nickel nanoparticle-graphene-foam nickel composite material used in catalysis, sensor, supercapacitor, batteries and dye adsorption applications. ADVANTAGE - The method enables simple preparation of nickel nanoparticle-graphene-foam nickel composite material. The nickel nanoparticles are uniform in size and stably distributed on the surface of the graphene-based foam nickel matrix material, and do not agglomerate easily. DETAILED DESCRIPTION - Preparation of nickel nanoparticle-graphene-foam nickel composite material involves washing foam nickel with acetone, ethanol and deionized water to remove surface oxide layer, drying, heat-treating foamed nickel in quartz tube, annealing, adding methane and hydrogen to grow graphene, rapidly reducing, cooling to room temperature to obtain foam nickel material covered with graphene to form graphene-foam nickel base material and carrying out current deposition using graphene-foam nickel base material as working electrode, platinum as counter electrode, silver-silver chloride as reference electrode and nickel sulfate-sulfuric acid mixed solution as electrolyte.