• 专利标题:   Preparation of two dimensional molybdenum disulfide and three dimensional graphene composite material includes pressing foam metal in sheet, performing chemical vapor deposition on foamed metal foil, annealing, soaking and rinsing.
  • 专利号:   CN107359327-A
  • 发明人:   NING J, LI A, HAO Y, ZHANG J, WANG D, CHEN J, DONG J, CHENG H
  • 专利权人:   UNIV XIDIAN
  • 国际专利分类:   B82Y040/00, H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN107359327-A 17 Nov 2017 H01M-004/36 201779 Pages: 9 Chinese
  • 申请详细信息:   CN107359327-A CN10522149 30 Jun 2017
  • 优先权号:   CN10522149

▎ 摘  要

NOVELTY - Preparation of two dimensional molybdenum disulfide and three dimensional graphene composite material comprises pressing 8-16 mm foam metal in 0.2-0.5 mm sheet, removing oil stain and metal oxide layer, using carbon source gas as gaseous reactant, performing chemical vapor deposition on foamed metal foil, placing in tube furnace, annealing, soaking two dimensional graphene, two dimensional metal molybdenum disulfide and metal foam in 0.8-1.2 M ferric chloride solution and 1.5-2.5 M hydrochloric acid solution, rinsing with deionized water, soaking and removing foam metal part. USE - Method of preparing two dimensional molybdenum disulfide and three dimensional graphene composite material (claimed). ADVANTAGE - The method is simple and improves lattice integrity, stability, capacity and cycle efficiency. DETAILED DESCRIPTION - Preparation of two dimensional molybdenum disulfide and three dimensional graphene composite material comprises pressing 8-16 mm foam metal in 0.2-0.5 mm sheet, removing oil stain and metal oxide layer, using carbon source gas as gaseous reactant, performing chemical vapor deposition on foamed metal foil, placing in tube furnace, annealing, soaking two dimensional graphene, two dimensional metal molybdenum disulfide and metal foam in 0.8-1.2 M ferric chloride solution and 1.5-2.5 M hydrochloric acid solution , rinsing with deionized water every 2-3 hours, soaking for 8-12 hours and removing foam metal part.