▎ 摘 要
NOVELTY - Three-dimensional stacked body reinforced titanium-based composite material is claimed. The reinforcement of composite material is three-dimensional accumulation; three-dimensional stacked body is formed by stacking two-dimensional graphene, array of silicon oxide nanotubes grown on surface of two-dimensional graphene sheet, and one-dimensional titanium oxide nanowires aligned in outermost layer; matrix of composite material is titanium or titanium alloy, and mass ratio between reinforcement and matrix is 1:2-4. USE - Used as three-dimensional stacked body reinforced titanium-based composite material. ADVANTAGE - The reinforcement composite material: has high strength, excellent interface with matrix, excellent thermal stability, improved mechanical properties and low production cost; and overcomes problems of high preparation cost of titanium-based composite material, poor mechanical properties, and poor high temperature resistance in existing art. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing three-dimensional stacked body-reinforced titanium-based composite material comprising (i) dispersing graphene nanosheets in ethanol to obtain graphene nanosheet dispersion, dissolving sophorolipid and bis(hydroxyethyl)methyl dodecylammonium chloride in mixture of ethanol and water in a volume ratio of 2:1, mixing dispersion liquid and mixed liquid, adding into three-necked flask and stirring at 50 degrees C for 1 hour, cooling to room temperature, adding ethyl orthosilicate dropwise, stirring for 3-5 hours, filtering, washing filtered solid and drying, placing dried powder in muffle furnace and calcining at 500 degrees C for 3 hours to obtain graphene/silicon oxide nanotube array composite, (ii) dissolving titanium tetrachloride in ethanol, stirring and mixing, adding hydrochloric acid solution dropwise, stirring for 10 minutes, then adding deionized water and stirring to obtain sol, stirring and mixing prepared sol and graphene/silica nanotube array composite, then adding tetrabutylammonium hydroxide, stirring at 50 degrees C for 5 hours, filtering, washing resulting precipitate and drying, then sintering at 500 degrees C for 2-4 hours to obtain three-dimensional stack, and (iii) mixing three-dimensional stack, base powder and ethanol, stirring and mixing at room temperature for 2-3 hours, then drying to obtain mixed powder, placing mixed powder in graphite mold using vacuum hot pressing sintering process to obtain three-dimensional stacked body reinforced titanium-based composite material.