• 专利标题:   Preparing oil sludge treatment agent comprises introducing cyclodextrin into modified liquid for modified stirring treatment, sending hybrid rectorite into silane coupling agent, mixing modified cyclodextrin, organic nano montmorillonite and hybrid rectorite, and blending.
  • 专利号:   CN113813929-A
  • 发明人:   QI Y, LIU Z, QI B
  • 专利权人:   PANJIN FURUIDA ENVIRONMENTAL PROTECTION TECHNOLOGY CO LTD
  • 国际专利分类:   B01J020/24, B01J020/30, C02F101/30, C02F011/00, C08B037/00
  • 专利详细信息:   CN113813929-A 21 Dec 2021 B01J-020/24 202220 Chinese
  • 申请详细信息:   CN113813929-A CN10733693 30 Jun 2021
  • 优先权号:   CN10733693

▎ 摘  要

NOVELTY - Preparing oil sludge treatment agent comprises (i) introducing cyclodextrin into modified liquid for modified stirring treatment, sending the nanometer montmorillonite into 3-glycidoxypropyltrimethoxysilane for low speed stirring, finishing stirring, water washing, drying to obtain the organic nanorubber-keling; (iii) introducing rectorite to the dispersion for stirring and dispersing, stirring, performing ultrasonic treatment ultrasonic power is 200-500 W for 30-40 min, ending the ultrasonic to obtain the hybrid rectorite, (iv) sending hybrid rectorite into the silane coupling agent for ultrasonic dispersing for 20-30 minutes, the ultrasonic power is 100- 500 W, finishing the ultrasonic, heating at 75-85 degreesC, washing and drying; (v) mixing the modified cyclodextrin, organic nano montmorillonite in (ii) and hybrid rectorite of (iv) together, the blending speed is 500-1000 revolutions/minutes, the blending time is 20-30 minutes to obtain the sludge treatment agent. USE - The method is useful for preparing oil sludge treatment agent. DETAILED DESCRIPTION - Preparing oil sludge treatment agent comprises (i) introducing cyclodextrin into modified liquid for modified stirring treatment, rotating at speed of 100- 500 revolutions/minutes for 30-40 minutes, modifying at 60-100 degrees Celsius, rotating to the organic agent for high speed stirring for 20-30 minutes, high speed stirring at speed of 600- 1200 revolutions/minutes, stirring to obtain the modified cyclodextrin, (ii) sending the nanometer montmorillonite into 3-glycidoxypropyltrimethoxysilane for low speed stirring, low speed stirring 50-100 revolutions/minutes, the stirring time is 30-40 minutes, stirring temperature is 50-100degrees Celsius, finishing stirring, water washing, drying to obtain the organic nano rubber-keling; (iii) introducing rectorite to the dispersion for stirring and dispersing, stirring at 70-100degrees Celsius, stirring time is 20-30 minutes, performing ultrasonic treatment ultrasonic power is 200-500 W for 30-40 min, ending the ultrasonic to obtain the hybrid rectorite, (iv) sending hybrid recto rite into the silane coupling agent for ultrasonic dispersing for 20-30 minutes, the ultrasonic power is 100- 500 W, finishing the ultrasonic, heating at 75-85 degreesC, washing and drying; (v) mixing the modified cyclodextrin, organic nano montmorillonite in (ii) and hybrid rectorite of (iv) together, the blending speed is 500-1000 revolutions/minutes, the blending time is 20-30 minutes to obtain the sludge treatment agent. An INDEPENDENT CLAIM is also included for use method of oil sludge treatment agent comprises introducing sludge treatment agent into the sludge, stirring at a speed of 100-200 revolutions/minutes for 20 minutes, heating to 60-70 degreesC at a rate of 1-5 degreesC/minute, incubating for 10-20minutes, cooling to 45 degreesC, warming for 30-50 minutes, and stirring at a speed of 400-600 revolutions/minutes for 20-30 minutes.