• 专利标题:   Synthesizing stannous sulfide/graphene cathode material by one-step solid phase method comprises mixing organotin compound and sulfur source by grinding, heating mixture in vacuum or argon atmosphere to obtain stannous sulfide/graphene,.
  • 专利号:   CN115411239-A
  • 发明人:   ZHAO C, GAO S, JIAN J, WANG X, LI H, WANG H, NIE P, CHANG L
  • 专利权人:   UNIV JILIN NORMAL
  • 国际专利分类:   B82Y030/00, B82Y040/00, H01M010/0525, H01M004/36, H01M004/58, H01M004/583
  • 专利详细信息:   CN115411239-A 29 Nov 2022 H01M-004/36 202306 Chinese
  • 申请详细信息:   CN115411239-A CN10817354 12 Jul 2022
  • 优先权号:   CN10817354

▎ 摘  要

NOVELTY - Synthesizing stannous sulfide/graphene cathode material by one-step solid phase method comprises (i) mixing uniformly an organotin compound and a sulfur source by grinding; the mass ratio of the organotin compound to the sulfur source is 1: (0.5-4), (ii) heating the mixture from room temperature to 600-800℃ at a heating rate of 2-5℃ minutes -1 in a vacuum or argon atmosphere, and maintaining the temperature for 2-5 hours to obtain stannous sulfide/graphene, stannous sulfide/graphene is composed of stannous sulfide particles and graphene sheets, the morphology of the stannous sulfide/graphene is a flower-shaped spherical structure formed by gathering nanosheets, and the diameter of the particles is 7-8 microns. USE - The method is useful for synthesizing stannous sulfide/graphene cathode material by one-step solid phase method. ADVANTAGE - The method has high purity, has excellent electrochemical performance in the lithium ion batteries, is simple, has positive meaning for widening the selection range, is low cost and has wide application prospects.