• 专利标题:   Preparing sewage treatment adsorption composite film containing graphene oxide comprises e.g. dispersing graphene oxide in water, and adding 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride and N-hydroxysuccinimide.
  • 专利号:   CN108837817-A
  • 发明人:   CHEN Q
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   B01J020/28, B01J020/20, B01J020/30, C02F001/28
  • 专利详细信息:   CN108837817-A 20 Nov 2018 B01J-020/28 201902 Pages: 9 Chinese
  • 申请详细信息:   CN108837817-A CN10683816 28 Jun 2018
  • 优先权号:   CN10683816

▎ 摘  要

NOVELTY - Preparing sewage treatment adsorption composite film containing graphene oxide comprises e.g. (1) dispersing graphene oxide in water, adding 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride and N-hydroxysuccinimide, carrying ultrasonic treatment for 50-80 minutes, suction filtering, drying to obtain surface activated graphene oxide; (2) dissolving the pore-forming agent in water, adding the surface-activated graphene oxide obtained in the step (1), stirring, filtering and drying to obtain graphene oxide powder supporting pore-forming agent; (3) uniformly dispersing the graphene oxide powder supporting pore-forming agent obtained in the step (2) in the solution of organic base film material, continuously stirring, adding defoaming agent and thickener to form viscous membrane casting solution; and (4) uniform coating the viscous membrane casting solution on base, removing solvent by heating, allowing to stand the base film to precipitate and solidify. USE - The method is useful for preparing sewage treatment adsorption composite film containing graphene oxide. ADVANTAGE - The composite film: has high filtration efficiency on water treatment, good sewage treatment effect, long service life, pollution resistance and toughness property; is simple to prepare. DETAILED DESCRIPTION - Preparing sewage treatment adsorption composite film containing graphene oxide comprises (1) dispersing graphene oxide in water, adding 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride and N-hydroxysuccinimide, carrying ultrasonic treatment for 50-80 minutes, suction filtering, drying to obtain surface activated graphene oxide; (2) dissolving the pore-forming agent in water, adding the surface-activated graphene oxide obtained in the step (1), stirring for 20-30 minutes, filtering and drying to obtain graphene oxide powder supporting pore-forming agent; (3) uniformly dispersing the graphene oxide powder supporting pore-forming agent obtained in the step (2) in the solution of organic base film material, continuously stirring, adding defoaming agent and thickener to form viscous membrane casting solution; and (4) uniform coating the viscous membrane casting solution on base, removing solvent by heating, allowing to stand the base film to precipitate and solidify, re-water washing and dissolving the pore-forming agent, to obtain water-treated adsorption film having nano-scale microporous structure. An INDEPENDENT CLAIM is also included for preparing the sewage treatment adsorption composite film containing graphene oxide is prepared by above mentioned method.