• 专利标题:   Preparation of nickel-graphene composite lithium battery material, involves adding graphene oxide to deionized water, ultrasonically dispersing, adding nickel nitrate solution, stirring, adding mixed lye and controlling reaction temperature.
  • 专利号:   CN108987716-A
  • 发明人:   SHEN X
  • 专利权人:   AOYANG GROUP CO LTD
  • 国际专利分类:   H01M004/36, H01M004/52, H01M004/62
  • 专利详细信息:   CN108987716-A 11 Dec 2018 H01M-004/36 201912 Pages: 5 Chinese
  • 申请详细信息:   CN108987716-A CN10813781 23 Jul 2018
  • 优先权号:   CN10813781

▎ 摘  要

NOVELTY - The preparation method of nickel-graphene composite lithium battery material involves (1) adding graphene oxide to deionized water, and ultrasonically dispersing for 1-2 hours to obtain graphene oxide suspension with concentration of 0.5-1.5 mg/mL, (2) adding nickel nitrate solution to the graphene oxide suspension, uniformly stirring, adding mixed lye while stirring, controlling the reaction temperature of the water bath at 50-60 degrees C, where the dripping speed of the mixed lye is 1-2 drops per second, and leaving still after finishing the reaction to obtain mixture containing nickel hydroxide, (3) taking the obtained mixture containing nickel hydroxide as a crystal seed, continuously dripping the mixed lye, stopping the reaction when the particle size of the nickel hydroxide reaches the requirement, vacuum filtering, washing with deionized water and absolute ethyl alcohol until neutral, and vacuum drying. USE - Preparation method of nickel-graphene composite lithium battery material. ADVANTAGE - The method enables preparation of nickel-graphene composite lithium battery material with fast reaction speed, uniform heating, short crystallization time, and high yield. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for nickel-graphene composite lithium battery material, which comprises nickel hydroxide and graphene in a mass ratio of (5-10):1.