• 专利标题:   Lithium ion battery cathode material comprises molybdenum disulfide/graphene composite material having structure of molybdenum disulfide particle that is perpendicular to graphene surface.
  • 专利号:   CN105591088-A, CN105591088-B
  • 发明人:   LI Z, XIA Q, ZHAO H, ZHANG Z, TENG Y
  • 专利权人:   UNIV BEIJING SCI TECHNOLOGY, UNIV BEIJING SCI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN105591088-A 18 May 2016 H01M-004/36 201660 Pages: 9 Chinese
  • 申请详细信息:   CN105591088-A CN10166713 22 Mar 2016
  • 优先权号:   CN10166713

▎ 摘  要

NOVELTY - A lithium ion battery cathode material comprises molybdenum disulfide/graphene composite material having a structure of molybdenum disulfide particle that is perpendicular to the graphene surface. USE - Lithium ion battery cathode material. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the preparation of lithium ion battery cathode material comprising: (A) dissolving molybdenum salt with sulfur in deionized water and stirring to form a first clear solution; weighing and adding the polyvinylpyrrolidone to the clarified first solution, stirring constantly to completely dissolve to obtain a second clear solution; adding an acid, adjusting the pH value of the second clear solution using an acid, adding graphene oxide, and carrying out ultrasound to obtain a uniform mixed solution, where the concentration of molybdenum is 6x 10-3 to 3x 10-1 mol/l, the concentration of the sulfur source is 2x 10-2 to 3 mol/l, and the concentration of polyvinylpyrrolidone is 4x 10-6 to 4x 10-4 mol/l; (B) adding the mixed solution with water in the autoclave lined reaction for 6-24 hours at a certain temperature to give the product; (C) washing the product with deionized water and ethanol, and dried in vacuum to obtain a powder precursor; and (D) carrying out heat treatment of the precursor powder under inert gas for 1-3 hours, and cooling to room temperature to obtain a lithium-ion battery anode material.