• 专利标题:   Method for preparing graphene-metal oxide electrode material, involves mixing graphene, dispersant and dilute sulfuric acid solution, homogenizing and dispersing, followed by drying composite film material.
  • 专利号:   CN107731353-A, CN107731353-B
  • 发明人:   SHAO G
  • 专利权人:   FOSHAN HUICHUANG ZHENGYUAN NEW MATERIALS, CECEP TANGSHAN ENVIRONMENTAL EQUIP CO, WU X
  • 国际专利分类:   H01B013/00, H01B005/14
  • 专利详细信息:   CN107731353-A 23 Feb 2018 H01B-005/14 201825 Pages: 7 Chinese
  • 申请详细信息:   CN107731353-A CN10940631 11 Oct 2017
  • 优先权号:   CN10940631

▎ 摘  要

NOVELTY - A graphene-metal oxide electrode material preparing method involves mixing graphene, dispersant and dilute sulfuric acid solution, homogenizing and dispersing to prepare a graphene emulsion. The graphene emulsion is sprayed on the surface of the polyethylene film to form a graphene surface layer. The graphene surface layer is dried, followed by spraying the metal mixture on the graphene surface film at a high speed to form composite film material, and drying the composite film material by argon gas to obtain the finished product. USE - Method for preparing graphene-metal oxide electrode material. ADVANTAGE - The method enables preparing graphene-metal oxide electrode material with good performance, good application prospect, and improved bending strength and fracture toughness. DETAILED DESCRIPTION - A graphene-metal oxide electrode material preparing method involves mixing graphene, dispersant and 7.5% dilute sulfuric acid solution, homogenizing and placing in an ultrasonic disperser for ultrasonic dispersion for 2-4 hours to prepare a graphene emulsion. The graphene emulsion is sprayed on the surface of the polyethylene film to form a graphene surface layer. The graphene surface layer is dried by argon gas, followed by mixing 2-3 parts magnesium powder, 1-2 parts nickel oxide, 2-3 parts magnesium carbonate, 1-2 parts copper powder, 1-3 parts titanium dioxide and 1-3 parts tri-n-octylphosphine oxide, adding into pipe type reaction furnace heating refining at 750-760 degrees C, adding 4-5 parts acetone aldehyde and pressurizing to 2.5 MPa for 5 hours to obtain metal mixture, spraying the metal mixture on the graphene surface film at a high speed to form composite film material, and drying the composite film material by argon gas to obtain the finished product.