• 专利标题:   Preparation of oil-water separation type sodium alginate/graphene oxide composite aerogel used in marine application, involves dissolving sodium alginate in deionized water, and stirring to prepare sodium alginate solution.
  • 专利号:   CN106853296-A, CN106853296-B
  • 发明人:   ZHANG H, LI Y, LU Z, ZHENG D, HUANG L, CHEN L
  • 专利权人:   UNIV FUJIAN AGRIC FORESTRY, UNIV FUJIAN AGRIC FORESTRY
  • 国际专利分类:   B01D017/022, B01J013/00, C08J003/075, C08J009/28, C08J009/40, C08L005/04
  • 专利详细信息:   CN106853296-A 16 Jun 2017 B01D-017/022 201756 Pages: 11 Chinese
  • 申请详细信息:   CN106853296-A CN11263274 30 Dec 2016
  • 优先权号:   CN11263274

▎ 摘  要

NOVELTY - The preparation of oil-water separation type sodium alginate/graphene oxide composite aerogel, involves dissolving sodium alginate in deionized water, magnetic stirring at 800-1200 rpm to prepare sodium alginate solution with concentration of 1-4 wt.%, ultrasonically treating 0.5-3 wt.% graphene oxide suspension for 10-20 minutes, adding to sodium alginate solution, magnetic stirring to obtain sodium alginate/graphene oxide dispersion, and placing vessel containing sodium alginate/graphene oxide dispersion in freeze-drying system for freeze-drying. USE - Preparation of oil-water separation type sodium alginate/graphene oxide composite aerogel (claimed) used in marine application. ADVANTAGE - The method enables preparation of oil-water separation type sodium alginate/graphene oxide composite aerogel with high porous structure, high separation efficiency, high salt tolerance, high flexibility, high mechanical strength, excellent oil resistance, and high reuse ability. DETAILED DESCRIPTION - The preparation of oil-water separation type sodium alginate/graphene oxide composite aerogel, involves dissolving sodium alginate in deionized water, magnetic stirring at 800-1200 rpm, gradually reducing the stirring speed to 500 rpm after 1-2 hours until becomes transparent solution to prepare sodium alginate solution with concentration of 1-4 wt.%, ultrasonically treating 0.5-3 wt.% graphene oxide suspension for 10-20 minutes, adding to sodium alginate solution, magnetic stirring at 1200-2000 rpm for not less than 2 hours to obtain sodium alginate/graphene oxide dispersion, and placing vessel containing sodium alginate/graphene oxide dispersion in freeze-drying system for freeze-drying. The mass ratio of graphene oxide to sodium alginate is 0.5:10-1:10. An INDEPENDENT CLAIM is included for oil-water separation type sodium alginate/graphene oxide composite aerogel.