• 专利标题:   Microwave-assisted sodium citrate reduction method for preparing graphene comprises using Hummers method to prepare graphite oxide, dispersing in deionized water, ultrasonically dispersing and reacting with sodium citrate.
  • 专利号:   CN102976315-A
  • 发明人:   YAN H, MAO K, LI S, FENG Y, LIU C
  • 专利权人:   UNIV NORTHWESTERN POLYTECHNICAL
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102976315-A 20 Mar 2013 C01B-031/04 201367 Pages: 7 Chinese
  • 申请详细信息:   CN102976315-A CN10525178 10 Dec 2012
  • 优先权号:   CN10525178

▎ 摘  要

NOVELTY - A microwave-assisted sodium citrate reduction method for preparing graphene comprises using Hummers method to prepare 0.05-0.3 g graphite oxide and dispersing in 200 mL deionized water, and ultrasonically dispersing at 210-300 W for 40-80 minutes; adding 1-30 g sodium citrate, putting in microwave reactor, and reacting at 70-95 degrees C for 60 seconds at stirring speed of 600 revolutions/minute (rpm); and cooling to room temperature, centrifuging at 13000 rpm and 3 times cleaning, freezing and drying to obtain graphene. USE - Method of microwave-assisted sodium citrate reduction for preparing graphene (claimed). ADVANTAGE - The method is fast and energy-saving, has environmental protection and high efficiency, prepares uniform size distribution and excellent electrical performance graphite, and provides technical assurance for application of graphite. DESCRIPTION OF DRAWING(S) - The drawing is a schematic diagram illustrating a microwave-assisted sodium citrate reduction method for preparing graphene.