• 专利标题:   Preparing rod-shaped cobalt tetraoxide/graphene nano composite material comprises e.g. mixing graphite flakes, sodium nitrate and concentrated sulfuric acid, adding potassium permanganate, stirring, washing, freeze-drying, and calcining.
  • 专利号:   CN110416519-A
  • 发明人:   LV C, LU J, GUO J, ZHANG L, QIN Y, WANG C
  • 专利权人:   UNIV BENGBU
  • 国际专利分类:   B82Y030/00, H01M010/0525, H01M004/36, H01M004/52, H01M004/62
  • 专利详细信息:   CN110416519-A 05 Nov 2019 H01M-004/36 201987 Pages: 8 Chinese
  • 申请详细信息:   CN110416519-A CN10698955 31 Jul 2019
  • 优先权号:   CN10698955

▎ 摘  要

NOVELTY - Preparing rod-shaped cobalt tetraoxide/graphene nano composite material comprises (1) mixing graphite flakes, sodium nitrate and concentrated sulfuric acid for 30 minutes to obtain a mixture a, (2) under the condition of ice water bath, adding potassium permanganate to the mixture a obtained in the step (1), stirring for 12 hours, adding deionized water, stirring for 12 hours, stirring with hydrogen peroxide for 24 hours to obtain mixture b, (3) washing mixture b with distilled water for 5-6 times, and freeze-drying to obtain graphene oxide, (4) uniformly mixing cobalt nitrate, urea, and graphene oxide in 40 ml deionized water, washing and heating to obtain solid product c, and (5) freeze-drying solid product c, calcining under argon atmosphere to obtain nanorod-shaped cobalt tetraoxide/graphene composite material. USE - The method is useful for preparing rod-shaped cobalt tetraoxide/graphene nano composite material. ADVANTAGE - The method is simple. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for nanorod-shaped cobalt tetraoxide/graphene nano composite material.