• 专利标题:   Nano-modified epoxy resin with high impact resistance and high elastic modulus for reinforced carbon fiber hot-melt prepreg comprises e.g. liquid epoxy resin, semi-solid epoxy resin, solid epoxy resin, graphene, fumed silica, nano toughening agent, wetting and dispersing agent, and accelerator.
  • 专利号:   CN114085489-A
  • 发明人:   QIN L, QIN J
  • 专利权人:   SHENCAI TECHNOLOGY SHENZHEN CO LTD
  • 国际专利分类:   C08J005/04, C08J005/24, C08K003/04, C08K007/06, C08K007/26, C08L063/00
  • 专利详细信息:   CN114085489-A 25 Feb 2022 C08L-063/00 202268 Chinese
  • 申请详细信息:   CN114085489-A CN11599644 29 Dec 2020
  • 优先权号:   CN11599644

▎ 摘  要

NOVELTY - Nano-modified epoxy resin with high impact resistance and high elastic modulus for reinforced carbon fiber hot-melt prepreg comprises 20-30 pts. wt. liquid epoxy resin, 10-20 pts. wt. semi-solid epoxy resin, 50-60 pts. wt. solid epoxy resin, 0.1-0.5 pts. wt. graphene, 1-3 pts. wt. fumed silica, 0.2-0.5 pts. wt. nano toughening agent, 1-3 pts. wt. wetting and dispersing agent, 6-12 pts. wt. latent curing agent, 1-3 pts. wt. accelerator, and 1-5 pts. wt. coupling agent. The nano toughening agent comprises nano-scale titanium-based compounds. The particle size of the nano-scale titanium-based compound is less than 50 nm. The mass percentage of the nano-scale titanium-based compound is not more than 10%. USE - Used as nano-modified epoxy resin with high impact resistance and high elastic modulus for reinforced carbon fiber hot-melt prepreg. ADVANTAGE - The nano-modified epoxy resin has high mechanical properties and guaranteed quality. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing the nano-modified epoxy resin, comprising (S1) mixing liquid epoxy resin, semi-solid epoxy resin and solid epoxy resin, and stirring at 150-160degrees Celsius and 200-500 revolutions per minute for 55-65 minutes to prepare a mixed epoxy resin, (S2) cooling the mixed epoxy resin to 95-105degrees Celsius, adding nano toughening agent, and wetting and dispersing agent, dispersing at 1450-1500 revolutions per minute for 5-7 minutes to obtain intermediate product A, (S3) adding graphene, fumed silica, and latent curing agent to intermediate product A, and dispersing at 95-105degrees Celsius and 1450-1500 revolutions per minute for 7-9 minutes to obtain intermediate product B, and (S4) cooling the intermediate product B to 75-85degrees Celsius, adding accelerator and coupling agent, and dispersing at 1450-1500 revolutions per minute for 5-7 minutes to obtain nano-modified epoxy resin for hot melt method.