• 专利标题:   Manufacture of graphene/molybdenum disulfide nanocomposite material involves dissolving sodium molybdate in aqueous ethanol solution, further reacting with sodium thiocyanate, sodium chloride and oxidized graphene, filtering and drying.
  • 专利号:   CN102796590-A, CN102796590-B
  • 发明人:   LI C, TANG G, TANG H, WU K, JI X
  • 专利权人:   UNIV JIANGSU
  • 国际专利分类:   C10M125/22, C10N030/06
  • 专利详细信息:   CN102796590-A 28 Nov 2012 C10M-125/22 201332 Pages: 8 Chinese
  • 申请详细信息:   CN102796590-A CN10303392 24 Aug 2012
  • 优先权号:   CN10303392

▎ 摘  要

NOVELTY - Sodium molybdate is dissolved in a mixed solution of ethanol and water to form a solution. To obtained solution, sodium thiocyanate and sodium chloride are dissolved. Oxidized graphene nanoflakes are ultrasonically dispersed in obtained solution and then filtered. The obtained filtrate is heated in stainless steel reactor, cooled to room temperature, filtered and centrifuged. The obtained product is washed using deionized water and absolute ethyl alcohol, and dried in nitrogen-hydrogen atmosphere, to obtain graphene/molybdenum disulfide nanocomposite material. USE - Manufacture of graphene/molybdenum disulfide nanocomposite material. DETAILED DESCRIPTION - Sodium molybdate is dissolved in a mixed solution of ethanol and water to form a solution (0.02-0.05 mol/L). To obtained solution, sodium thiocyanate and sodium chloride are dissolved. The mass ratio of sodium thiocyanate and sodium molybdate is 2:1-4:1. The mass ratio of sodium chloride and sodium molybdate is 2:1-4:1. Oxidized graphene nanoflakes are ultrasonically dispersed in obtained solution and then filtered. The mass ratio of oxidized graphene and sodium molybdate is 1:1-4:1. The obtained filtrate is heated in stainless steel reactor at 180-220 degrees C for 24-48 hours. The obtained solution is cooled to room temperature, filtered and centrifuged. The obtained product is washed using deionized water and absolute ethyl alcohol, and dried by heating at 800-900 degrees C for 2 hours in nitrogen-hydrogen atmosphere, to obtain graphene/molybdenum nanocomposite material. The graphene/molybdenum disulfide nanocomposite material has hollow tubular structure having length of 1-3 mu m and diameter of 200-500 nm.