• 专利标题:   Preparation of aqueous epoxy resin emulsion for paint, involves stirring epoxy resin and propylene glycol methyl ether, mixing with emulsifier, polyethylene glycol, boron trifluoride and modified graphene, dripping water and reacting.
  • 专利号:   CN111808300-A
  • 发明人:   CHENG H
  • 专利权人:   CHENG H
  • 国际专利分类:   C08J003/03, C08K013/06, C08K003/04, C08K003/38, C08K009/02, C08K009/04, C08L063/00, C08L071/02
  • 专利详细信息:   CN111808300-A 23 Oct 2020 C08J-003/03 202094 Pages: 8 Chinese
  • 申请详细信息:   CN111808300-A CN10680485 15 Jul 2020
  • 优先权号:   CN10680485

▎ 摘  要

NOVELTY - Preparation of graphene-based aqueous epoxy resin emulsion involves weighing 10-15 pts. wt. modified graphene, 3-5 pts. wt. emulsifier, 35-50 pts. wt. epoxy resin, 5-10 pts. wt. polyethylene glycol, 120-150 pts. wt. propylene glycol methyl ether, 20-30 pts. wt. deionized water, 1-2 pts. wt. boron trifluoride and 1-3 pts. wt. leveling agent, adding epoxy resin into beaker containing propylene glycol methyl ether, heating in water bath at 60-65 degrees C, stirring under constant speed until a transparent solution is formed, adding emulsifier and polyethylene glycol, stirring for 30 minutes, adding boron trifluoride and modified graphene, cooling to 30-35 degrees C, stirring at constant speed for 10 minutes, reacting at 85 degrees C for 2 hours, cooling to 60 degrees C, dripping deionized water for 1 hour, stirring and reacting at constant speed for 30 minutes, adding leveling agent and mixing. USE - Preparation of graphene-based aqueous epoxy resin emulsion for paint. ADVANTAGE - The prepared emulsion has excellent flame retardance and dispersibility in organic phase and aqueous solvent due to formation of three-dimensional structure, and can transfer heat and volatilize flammable gas volatilization to form carbon layer to protect paint matrix from burning.