• 专利标题:   Preparing a six-membered heterocyclic ring covalently modified graphene oxide/epoxy resin composite material comprises ultrasonically dispersing modified graphene oxide to acetone, adding epoxy resin, curing agent, molding, and drying.
  • 专利号:   CN110305448-A
  • 发明人:   MA L, ZHU Y, GUO S, ZHU X, XIN J, SHEN Y, LV B, ZHANG S, MU Y
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   C08K003/04, C08K009/02, C08K009/04, C08L063/00
  • 专利详细信息:   CN110305448-A 08 Oct 2019 C08L-063/00 201984 Pages: 26 Chinese
  • 申请详细信息:   CN110305448-A CN10622858 11 Jul 2019
  • 优先权号:   CN10622858

▎ 摘  要

NOVELTY - Preparing a six-membered heterocyclic ring covalently modified graphene oxide/epoxy resin composite material comprises adding a six-membered heterocyclic ring-modified graphene oxide to acetone, ultrasonically dispersing to obtain a mixed solution, where the ratio graphene oxide covalently modified by the six-membered heterocyclic ring to acetone is (0.033-0.036 g): (10-15 ml), adding an epoxy resin to the mixed solution, ultrasonically dispersing, drying to obtain an epoxy resin mixture, where the ratio of the epoxy resin to graphene oxide covalently modified by six-membered heterocyclic ring is (33-36): (0.033-0.036), adding a curing agent to the epoxy resin mixture, stirring, drying to obtain an epoxy resin mixture and pouring the epoxy resin mixture containing curing agent into the preheating mold, vacuum drying, solidifying to obtain a six-membered heterocyclic ring covalently modified graphene oxide/epoxy resin composite material. USE - The method is useful for preparing a six-membered heterocyclic ring covalently modified graphene oxide/epoxy resin composite material. ADVANTAGE - The method solve the problems of graphene having poor dispersibility and epoxy resin having poor compatibility; is highly economical and has small amount of covalently modified graphene oxide in the composite material, which greatly reduces the cost. DETAILED DESCRIPTION - Preparing a six-membered heterocyclic ring covalently modified graphene oxide/epoxy resin composite material comprises (1) adding a six-membered heterocyclic ring-modified graphene oxide to acetone, ultrasonically dispersing to obtain a mixed solution, where the ratio graphene oxide covalently modified by the six-membered heterocyclic ring to acetone is (0.033-0.036 g): (10-15 ml), (2) adding an epoxy resin to the mixed solution, ultrasonically dispersing, drying to obtain an epoxy resin mixture, where the ratio of the epoxy resin to graphene oxide covalently modified by six-membered heterocyclic ring is (33-36): (0.033-0.036), (3) adding a curing agent to the epoxy resin mixture, stirring, drying to obtain an epoxy resin mixture, where the ratio of the curing agent to epoxy resin is (10-11): (33-36) and (4) pouring the epoxy resin mixture containing curing agent into the preheating mold at 80 degrees C, vacuum drying to 80 degrees C at -30 kPa, solidifying to obtain a six-membered heterocyclic ring covalently modified graphene oxide/epoxy resin composite material.