• 专利标题:   Preparing composite material used in lithium ion battery, by ultrasonically treating mixed liquid containing lithium hydroxide and graphene, dripping tetrabutyl titanate, treating reaction solution and reacting precursor solution.
  • 专利号:   CN108134068-A
  • 发明人:   YU K, WANG Y, ZHANG X, CAO X, WANG Z, ZOU K
  • 专利权人:   UNIV JILIN, NALON BATTERY SHENZHEN CO LTD
  • 国际专利分类:   H01M004/36, H01M004/485, H01M004/62, H01M010/0525, B82Y030/00, B82Y040/00
  • 专利详细信息:   CN108134068-A 08 Jun 2018 H01M-004/36 201854 Pages: 14 Chinese
  • 申请详细信息:   CN108134068-A CN11421262 25 Dec 2017
  • 优先权号:   CN11421262

▎ 摘  要

NOVELTY - The method for preparing titanium dioxide-graphene oxide composite material involves (a) providing a mixed liquid containing lithium hydroxide and graphene, (b) ultrasonically treating the mixed liquid, dripping tetrabutyl titanate to obtain a reaction solution and ultrasonically treating the reaction solution for 1-4 hours to obtain a precursor solution, where the mass ratio of tetrabutyl titanate to lithium hydroxide is 1:3-1:7, (c) hydrothermally reacting the precursor solution at 100-200 degrees C for 12-120 hours, carrying out solid-liquid separation to obtain a solid, washing the solid, drying to obtain a product (i) and crushing the product (i), and (d) calcining the product (i) at 350-450 degrees C for 1-8 hours to obtain titanium dioxide-graphene oxide composite material. USE - Method is useful for preparing titanium dioxide-graphene oxide composite material, which is useful in a battery (all claimed), preferably lithium ion battery. ADVANTAGE - The titanium dioxide-graphene oxide composite material is simple to prepare, and improves discharge specific capacity and cycle stability of the lithium ion battery. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the titanium dioxide-graphene oxide composite material prepared by the above method.