• 专利标题:   Preparing strong alkaline graphene composite resin material, comprises carrying out microwave- and ultrasonic- treatment of monomer, and carrying out co-polymerization of monomers and graphene solution.
  • 专利号:   CN104558359-A
  • 发明人:   HE W, LI Y, YANG W, YU F
  • 专利权人:   SHANGHAI PETROCHEM TECHNOLOGY RES IN, CHINA PETROLEUM CHEM CORP
  • 国际专利分类:   B01J039/20, B01J041/14, B01J043/00, C08F002/00, C08F002/44, C08F212/14, C08F212/34, C08F212/36, C08F008/32, C08J003/00, C08K003/04, C08L025/18
  • 专利详细信息:   CN104558359-A 29 Apr 2015 C08F-212/14 201568 Pages: 9 Chinese
  • 申请详细信息:   CN104558359-A CN10512392 28 Oct 2013
  • 优先权号:   CN10512392

▎ 摘  要

NOVELTY - Preparing strong alkaline graphene composite resin material, comprises carrying out microwave- and ultrasonic- treatment of monomer, and carrying out co-polymerization of monomers and graphene solution, where the composite resin material includes (i) 75-90% polymerizable monomer, (b) 5-15% comonomer, (c) 0.1-5% grapheme, and (d) 0.1-10% initiator, and the polymerizable monomer is chloromethylstyrene, 4-(3-chloropropyl) styrene, 4-(3-bromopropyl) styrene, 4-(4-chlorobutyl) styrene, 4-(4-bromobutyl) styrene, 4-(5-chloro-pentyl) styrene or 4-(5-bromo-pentyl) styrene. USE - The method is useful for preparing strong alkaline graphene composite resin material (claimed). ADVANTAGE - The method is suitable for industrial production. DETAILED DESCRIPTION - Preparing strong alkaline graphene composite resin material, comprises carrying out microwave- and ultrasonic- treatment of monomer, and carrying out co-polymerization of monomers and graphene solution, where the composite resin material includes (i) 75-90% polymerizable monomer, (b) 5-15% comonomer, (c) 0.1-5% grapheme, and (d) 0.1-10% initiator, and the polymerizable monomer is chloromethylstyrene, 4-(3-chloropropyl) styrene, 4-(3-bromopropyl) styrene, 4-(4-chlorobutyl) styrene, 4-(4-bromobutyl) styrene, 4-(5-chloro-pentyl) styrene or 4-(5-bromo-pentyl) styrene, and the comonomer is ethylene glycol dimethacrylate, diallyl benzene, divinyl diphenyl methane or divinyl benzene, and the graphene used is mono-layered graphene, multi-layered graphene or graphene oxide, and the initiator is benzoyl peroxide, azobisisobutyronitrile, lauroyl peroxide or cumene hydroperoxide.