• 专利标题:   Preparation of carbon-copper-tin alloy cathode material involves dispersing carbon nanotubes to copper plating solution, applying direct current, dispersing carbon nanotubes and/or graphene to tin-plating solution, and heating.
  • 专利号:   CN103066252-A, CN103066252-B
  • 发明人:   CAO F, JIANG Z, MA Z, LEI W, ZHOU Y, CHENG J, ZHOU W, PAN Y
  • 专利权人:   UNIV XIANG TAN, UNIV XIANGTAN
  • 国际专利分类:   C25D015/00, C25D005/50, H01M004/134, H01M004/1395, H01M004/38, H01M004/62
  • 专利详细信息:   CN103066252-A 24 Apr 2013 H01M-004/38 201364 Pages: 10 Chinese
  • 申请详细信息:   CN103066252-A CN10562912 21 Dec 2012
  • 优先权号:   CN10562912

▎ 摘  要

NOVELTY - Carbon nanotubes are uniformly dispersed to copper plating solution, and direct current is applied on copper foil. The copper-carbon nanotubes composite coating layer is heated under protective atmosphere. Carbon nanotubes and/or graphene are uniformly dispersed to tin-plating solution and direct current is applied, to obtain tin-carbon nanotubes or tin-graphene or tin-carbon nanotubes-graphene composite coating. The resultant product is heated to obtain carbon-copper-tin alloy cathode material. USE - Preparation of carbon-copper-tin alloy cathode material (claimed). ADVANTAGE - The carbon-copper-tin alloy cathode material having excellent cyclic characteristics is manufactured by simple process. DETAILED DESCRIPTION - Carbon nanotubes are uniformly dispersed to copper plating solution, and direct current is applied on copper foil, to obtain copper-carbon nanotubes composite coating layer. The resultant product is heat treated under protective atmosphere. Carbon nanotubes and/or graphene are uniformly dispersed to tin-plating solution and direct current is applied, to obtain tin-carbon nanotubes or tin-graphene or tin-carbon nanotubes-graphene composite coating. The resultant product is heated to obtain carbon-copper-tin alloy cathode material. The content of carbon nanotubes with respect to copper plating solution is 2-8 g/L. The concentration of carbon nanotubes and/or graphene is 1-5 g/L.