• 专利标题:   Preparation of high-density multi-graphene gelling material involves ultrasonically dispersing graphite oxide solution, adding reducing agent, freeze-drying graphene hydrogel, molding, adding graphite oxide/reducing agent and recycling.
  • 专利号:   CN104817076-A, CN104817076-B
  • 发明人:   LI Z, BEI H, LIAO X
  • 专利权人:   UNIV JIANGNAN
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN104817076-A 05 Aug 2015 C01B-031/04 201604 Pages: 6 Chinese
  • 申请详细信息:   CN104817076-A CN10226952 06 May 2015
  • 优先权号:   CN10226952

▎ 摘  要

NOVELTY - Graphite oxide solution is ultrasonically dispersed uniformly, and reducing agent is added and heated to obtain graphene hydrogel. Obtained product is frozen-dried to obtain graphene gel (a). Obtained gel is added to mold with a needle puncture, and graphite oxide/reducing agent mixture is poured to obtain graphene gel (b). Obtained graphene gel (a) and graphene gel (b) are recycled to obtain high-density multi-graphene gelling material. USE - Preparation of high-density multi-graphene gelling material (claimed). ADVANTAGE - The method efficiently provides high-density multi-graphene gelling material having excellent mechanical strength, electroconductivity and elasticity. DETAILED DESCRIPTION - Graphite oxide solution is ultrasonically dispersed uniformly, and reducing agent is added and heated to obtain graphene hydrogel. The obtained product is frozen-dried to obtain graphene gel (a). The obtained gel is added to a mold with a needle puncture, and graphite oxide/reducing agent mixture is poured to obtain graphene gel (b). The obtained graphene gel (a) and graphene gel (b) are recycled to obtain high-density multi-graphene gelling material. The obtained gel is ultrasonically dispersed, and an adhesive solution is uniformly added. The resultant material is drip-coated on an electrode surface, dried and subjected to electrochemical workstation to test the electrochemical properties.