• 专利标题:   Preparation of lithium-sulfur battery material used as cathode material for lithium-sulfur battery, involves preparing biomass carbon material using discarded cigarette butts, reacting with graphene oxide, heating and adding sulfur powder.
  • 专利号:   CN108832084-A
  • 发明人:   WU R, XU H, LIU Y, HA Y
  • 专利权人:   UNIV FUDAN
  • 国际专利分类:   H01M004/36, H01M004/38, H01M004/62, H01M010/052
  • 专利详细信息:   CN108832084-A 16 Nov 2018 H01M-004/36 201903 Pages: 8 Chinese
  • 申请详细信息:   CN108832084-A CN10568459 05 Jun 2018
  • 优先权号:   CN10568459

▎ 摘  要

NOVELTY - The preparation of lithium-sulfur battery material involves (1) collecting discarded cigarette butts, ultrasonically washing with ethanol and water 3-5 times and drying at 60-100 degrees C for 2-24 hours to obtain biomass carbon material, (2) mixing 2-20 mg/mL graphene oxide and 10-50 mg biomass carbon material, stirring for 2-8 hours, taking out composite sample and freeze drying at -30--70 degrees C for 24-36 hours to obtain biomass carbon composite precursor with graphene oxide, (3) placing 20-70 mg prepared biomass carbon composite precursor with graphene oxide in porcelain boat, placing in tube furnace, purging with argon gas, heating at 600-1000 degrees C at rate of 2-5 degrees C/minute for 3-9 hours to obtain composite material, adding 200-400 mg sulfur powder to composite material and vacuum sealing or melting. USE - Preparation of lithium-sulfur battery material used as cathode material for lithium-sulfur battery (claimed). ADVANTAGE - The method enables large-scale preparation of lithium-sulfur battery material ensuring increased electrical conductivity, high battery specific capacity, excellent cycle stability and enhanced performance by simple, economical and environmentally-friendly process.