• 专利标题:   Method for making graphene composite for forming electrode in capacitor device, involves combining composition, fist salt with divalent cation and second salt with trivalent cation, and heating solution under solvothermal conditions.
  • 专利号:   WO2014101128-A1, US2015340171-A1, US9887046-B2
  • 发明人:   LI Z, YAN T, SUN X, LIU J, WANG G, GU Z
  • 专利权人:   UNIV JIANGNAN, LI Z, YAN T, SUN X, LIU J, WANG G, GU Z
  • 国际专利分类:   H01G009/042, B01J019/24, H01G011/38, C01B031/04, C01B032/192, H01B001/04, H01G011/32, H01G011/86
  • 专利详细信息:   WO2014101128-A1 03 Jul 2014 H01G-009/042 201446 Pages: 44 English
  • 申请详细信息:   WO2014101128-A1 WOCN087877 28 Dec 2012
  • 优先权号:   WOCN087877, US14758210

▎ 摘  要

NOVELTY - The method (100) involves reacting graphene oxide with reductive agent (120) to obtain a first composition. Chemical activation agent is reacted with reduced graphene oxide (130). A portion of particles is removed from the first composition (140) to obtain a second composition. The second composition is heated under reductive atmosphere (150) to obtain a third composition. The third composition, first salt with divalent cation and second salt with trivalent cation are combined (160). The second solution is heated under solvothermal conditions sufficient to obtain a graphene composite (170). USE - Method for making a graphene composite for forming an electrode in a graphene composite capacitor device (claimed). ADVANTAGE - The method enables heating the second solution under solvothermal conditions sufficient so as to obtain the graphene composite for forming the electrode in the graphene composite capacitor device in an efficient manner. DETAILED DESCRIPTION - The particles comprise a polyolefin, polystyrene and acrylic, silica. The salt comprises magnesium ion, zinc ion, copper ion, manganese ion, calcium ion, iron ion, aluminum iodide, chromium ion, Cobalt ion, Gallium ion, Cerium ion and Lanthanum ion. The graphene composite is combined with a binding medium and a conductive agent, where the binding medium is selected from a group consisting of PTFE, plastic, stainless steel, glass and ceramic, and the conductive agent is selected from a group consisting of acetylene black, polyaniline, polyoxyphenylene, polyphenylene sulfide, polythiophene, polyfuran, polypyrrole, polymethylpyrrole, polycarbozole and polyazulene. INDEPENDENT CLAIMS are also included for the following: (1) a graphene composite (2) a graphene composite capacitor device (3) a system for making a graphene composite. DESCRIPTION OF DRAWING(S) - The drawing shows a flow diagram illustrating a method for making a graphene composite. Method for making graphene composite (100) Step for reacting graphene oxide with reductive agent (120) Step for reacting chemical activation agent with reduced graphene oxide (130) Step for removing portion of particles from first composition (140) Step for heating second composition under reductive atmosphere (150) Step for combining third composition, first salt with divalent cation and second salt with trivalent cation (160) Step for heating second solution under solvothermal conditions sufficient to obtain graphene composite (170)