• 专利标题:   Preparation of composite material used for lithium ion battery involves processing graphene and metal ion compound, mixing iron, phosphorus, and lithium source, processing, adding carbon source, grinding, drying, sintering, and cooling.
  • 专利号:   CN105932254-A
  • 发明人:   HE P, SHEN Z, YANG S, ZHENG Y
  • 专利权人:   HUNAN LISHUN ENERGY TECHNOLOGY CO LTD
  • 国际专利分类:   H01M010/0525, H01M004/133, H01M004/136, H01M004/1393, H01M004/1397, H01M004/36, H01M004/58, H01M004/583
  • 专利详细信息:   CN105932254-A 07 Sep 2016 H01M-004/36 201680 Pages: 6 Chinese
  • 申请详细信息:   CN105932254-A CN10402290 08 Jun 2016
  • 优先权号:   CN10402290

▎ 摘  要

NOVELTY - Preparation of composite material comprises taking graphene and metal ion compound at ratio of 1:0.03-0.5, emulsifying for 1-2 hours at 40-60 degrees C, and spray drying at 300-400 degrees C; mixing with iron source compound, phosphorus source compound, and lithium source compound salt, grinding for 5-8 hours at 25-45 degrees C, and spray drying under inert gas protection for 100-200 degrees C; and adding carbon source compound at ratio of 1:0.03-0.15, grinding for 2-5 hours at 30-50 degrees C, spray drying under inert gas protection at 100-200 degrees C, grading, sintering for 6-10 hours, and cooling to room temperature. USE - Method for preparing composite material (claimed) used for lithium ion battery. ADVANTAGE - The composite material has high charging capacity, high charging and discharging efficiency to more than 98%, where standard state is more than 92%, and high tap density, increases lithium ion battery energy density and ion diffusion coefficient, and has high electric conductivity and high multiplying discharge circuit performance. DETAILED DESCRIPTION - Preparation of composite material comprises taking graphene and metal ion compound at ratio of 1:0.03-0.5, emulsifying for 1-2 hours at 40-60 degrees C, and spray drying at 300-400 degrees C; mixing with iron source compound, phosphorus source compound, and lithium source compound salt at ratio of 1:1.1:0.85-1.15:0.6-0.8, grinding for 5-8 hours at 25-45 degrees C, and spray drying under inert gas protection at 100-200 degrees C; and adding carbon source compound at ratio of 1:0.03-0.15, grinding for 2-5 hours at 30-50 degrees C, spray drying under inert gas protection at 100-200 degrees C, grading, sintering for 6-10 hours, and cooling to room temperature.