• 专利标题:   Method for preparing high specific surface graphene, involves placing solution in water bath at specific temperature to obtain reduced graphene and drying to solid, after adding vitamin C and Hans ester to suspension.
  • 专利号:   CN113620282-A
  • 发明人:   WU J, LI T, QUE M, CHEN L, SUN Y, SUN J
  • 专利权人:   UNIV SUZHOU SCI TECHNOLOGY
  • 国际专利分类:   C01B032/192
  • 专利详细信息:   CN113620282-A 09 Nov 2021 C01B-032/192 202203 Chinese
  • 申请详细信息:   CN113620282-A CN10908256 09 Aug 2021
  • 优先权号:   CN10908256

▎ 摘  要

NOVELTY - The method involves adding 15 mg/mL strong alkali aqueous solution to 10 mg/mL graphene oxide solution and mixing uniformly to obtain a suspension and the volume ratio of the strong alkali solution to the graphene oxide solution is 6:1 to 1:1. The solution is placed in a water bath at 85degrees Celsius-95degrees Celsius to react for 24-30 hours to obtain the reduced graphene and dried to a solid, after adding 0.1-0.4g vitamin C and 0.1g Hans ester 1,4-dihydropyridine to the suspension. The dried solid is washed in turn by ethanol and deionized water to obtain a final product. A strong base is selected from two of sodium hydroxide, potassium hydroxide, lithium hydroxide or calcium hydroxide. The graphite oxide is oxidized to obtain graphite oxide, and water is added ultrasonically to obtain the graphene oxide solution. USE - Method for preparing high specific surface graphene. ADVANTAGE - The specific surface area of the graphene is greater than 1000 m2/g and the cost is low. The environmental friendliness is high.