• 专利标题:   Preparation of graphene-doped tin-nickel alloy nanoparticles involves dissolving graphite oxide, tin salt and nickel salt in solvent, then adding hydrazine hydrate to obtained mixture, ultrasonically-treating and heating.
  • 专利号:   CN103934471-A, CN103934471-B
  • 发明人:   WEN M, WU Y, CHEN S
  • 专利权人:   UNIV TONGJI
  • 国际专利分类:   B22F001/00, B22F009/24
  • 专利详细信息:   CN103934471-A 23 Jul 2014 B22F-009/24 201468 Pages: 13 Chinese
  • 申请详细信息:   CN103934471-A CN10142745 11 Apr 2014
  • 优先权号:   CN10142745

▎ 摘  要

NOVELTY - Graphite oxide, tin salt and nickel salt are dissolved in a solvent, then hydrazine hydrate is added to obtained mixture, ultrasonically-treated, heated at 170-200 degrees C for 2-24 hours, centrifuged, and product is collected and washed, to obtain graphene-doped tin-nickel alloy nanoparticles. The mass ratio of graphite oxide and tin salt is 1:2-1:10. The mass of graphite oxide and nickel salt is 1:2-1:10. The mass ratio of tin salt and nickel salt is 1:5-5:1. The mass ratio of hydrazine hydrate and graphene oxide is 5:1-30:1. USE - Preparation of graphene-doped tin-nickel alloy nanoparticles (claimed). ADVANTAGE - The method efficiently and stably provides graphene-doped tin-nickel alloy nanoparticles with high purity, by simple process under mild reaction conditions.