• 专利标题:   Preparation of lubricating oil composite nano wearable additive by preparing brucite precursor and mixed system, adding i.e. molybdate and titanate, mixing with brucite precursor and graphene, reacting, adjusting pH and calcining.
  • 专利号:   CN107880972-A
  • 发明人:   WANG T
  • 专利权人:   WANG T
  • 国际专利分类:   C10M125/00, C10M125/02, C10M125/10, C10M125/26, C10N030/06
  • 专利详细信息:   CN107880972-A 06 Apr 2018 C10M-125/00 201828 Pages: 8 Chinese
  • 申请详细信息:   CN107880972-A CN11033815 30 Oct 2017
  • 优先权号:   CN11033815

▎ 摘  要

NOVELTY - Preparation of lubricating oil composite nano wearable additive comprises preparing brucite precursor by preparing interlayer anions nitrate (NO3-), plywood bivalent, trivalent cations with M2+/M3+ hydrotalcite precursor; reacting aluminum source and fatty amine in until to precipitate disappears, adding water soluble silicate, molybdate, organic titanate, mixing uniformly to obtain mixed system 1; adding brucite precursor and graphene in mixed system 1, reacting for 3-8 hours, adding acidic substance to adjust pH obtain product; calcining pre-product to obtain antiwear additive. USE - Lubricating oil composite nano wearable additive. ADVANTAGE - The additive is added with nano particles to uniformly disperse the wear-resistant particles in the system, have good integration into lubricating oil and improves anti-wear and extreme pressure performance of lubricating oil. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: (1) preparation of lubricating oil composite nano wearable additive comprises preparing brucite precursor by preparing interlayer anions of NO3-, plywood bivalent, trivalent cations with M2+/M3+ hydrotalcite precursor; reacting aluminum source and fatty amine in until to precipitate disappears completely, adding water soluble silicate, molybdate, organic titanate, mixing uniformly to obtain mixed system; adding brucite precursor and graphene in mixed system, reacting at 60-120 degrees C for 3-8 hours, adding acidic substance to adjust pH to 3-5 to obtain product; calcining pre-product in inert gas to obtain antiwear additive; and (2) preparation of hydrotalcite precursor comprising mixing M2+ and M3+ in aqueous solution, adding alkaline substance, adjusting pH to 10-11, crystallizing at 60-120 degrees C for 4-10 hours, and neutralizing by centrifugal-washing. M=metal; M2+=magnesium (II) ion, zinc (II) ion, copper (II) ion, nickel (II) ion, or cobalt (II) ion; and M3+=aluminum (III) ion, iron (III) ion or chromium (III) ion.