• 专利标题:   Preparation of graphene involves taking flake graphite, mixing with concentrated sulfuric acid, heating, carrying out ultrasonication, standing, separating, dehydrating, refluxing with hydrazine hydrate, cooling, filtering and drying.
  • 专利号:   CN103539110-A, CN103539110-B
  • 发明人:   HUANG S, LAI Q
  • 专利权人:   UNIV PANZHIHUA
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103539110-A 29 Jan 2014 C01B-031/04 201422 Pages: 10 Chinese
  • 申请详细信息:   CN103539110-A CN10534483 31 Oct 2013
  • 优先权号:   CN10534483

▎ 摘  要

NOVELTY - Preparation of graphene comprises taking flake graphite, mixing with concentrated sulfuric acid and potassium permanganate, heating, adding aqueous solution of hydrogen peroxide, stirring for 0.5-2 hours, filtering, washing with water until pH value is 6-7, formulating solid into 2-5 g/mL suspension, carrying out ultrasonication for 20-40 minutes, standing for 12-48 hours, separating, dehydrating until liquid volume is 1/3, concentrating, refluxing with hydrazine hydrate for 18-24 hours, cooling, filtering and drying. USE - Method for preparing graphene (claimed). ADVANTAGE - The product is highly efficient and has low cost.