• 专利标题:   Preparation of graphene paper by adding graphite oxide in solvent, treating, heating, pressurizing, filtering under vacuum, drying filter cake, peeling off filtrate, placing into inert atmosphere, preheating, heating, and cooling.
  • 专利号:   CN103833027-A
  • 发明人:   WANG Y, WU F, YUAN X, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103833027-A 04 Jun 2014 C01B-031/04 201452 Pages: 7 Chinese
  • 申请详细信息:   CN103833027-A CN10491207 27 Nov 2012
  • 优先权号:   CN10491207

▎ 摘  要

NOVELTY - Preparation of graphene paper comprises adding graphite oxide in solvent, preparing to concentration of 0.25-1 mg/ml graphite oxide solution, and ultrasonically treating to obtain uniformly dispersed graphene oxide suspension; placing into reaction kettle, sealing, heating, and pressurizing to obtain stable graphene suspension; filtering using microporous filter under vacuum, drying filter cake, and peeling off filtrate from the surface of microporous filter membrane; placing in an inert atmosphere, preheating to 200 degrees C for 5 minutes, heating to 500-1000 degrees C, and cooling for 0.5-2 hours. USE - Method for preparing graphene paper (claimed). ADVANTAGE - The method is easy, has high permeability and solubility of graphite and better dispersion, and avoids reduction of graphene.