• 专利标题:   Preparing graphene involves treating lignin with alkali then with metallic catalyst.
  • 专利号:   CN105439135-A, CN105439135-B
  • 发明人:   CHEN Q, CHEN B, ZENG J, YE R, LIN L
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD, LIN L
  • 国际专利分类:   B82Y040/00, C01B031/04, C01B032/184
  • 专利详细信息:   CN105439135-A 30 Mar 2016 C01B-031/04 201643 Pages: 6 English
  • 申请详细信息:   CN105439135-A CN11007072 30 Dec 2015
  • 优先权号:   CN11007072

▎ 摘  要

NOVELTY - Preparing of graphene involves mixing solution of an alkali lignin with a solid in mass ratio of 1:5-10. The solution is heated to 70-100 degrees C for 1-3 hours. The solution is filtered after alkali treatment, residue is washed and dried at 60-80 degrees C to obtain lignin. The obtained lignin is treated with catalyst, mixed thoroughly in high pressure homogenizer maintained at 20-100 MPa that causes cleavage of the carbon in a homogenizer to obtain a high energy state which is taken into an autoclave, filled with inert gas, at a rate of 0.1-1 MPa/seconds and mixture is heated at rate of 30-60 degrees C/minutes. USE - Method for preparing graphene (claimed). ADVANTAGE - The method enables to prepare graphene in simple, cost effective manner and graphene has wide market prospect. DETAILED DESCRIPTION - Preparing of graphene involves mixing solution of an alkali lignin with a solid in mass ratio of 1:5-10. The solution is heated to 70-100 degrees C for 1-3 hours. The solution is filtered after alkali treatment, residue is washed and dried at 60-80 degrees C to obtain lignin. The obtained lignin is treated with catalyst, mixed thoroughly in high pressure homogenizer maintained at 20-100 MPa that causes cleavage of the carbon in a homogenizer to obtain a high energy state which is taken into an autoclave, filled with inert gas, at a rate of 0.1-1 MPa/seconds and mixture is heated at rate of 30-60 degrees C/minutes to 500-800 degrees C at 20- 50 MPa to obtain graphene.