• 专利标题:   Preparation of graphene nanobelt/poly(methyl methacrylate) micro-foamed nanocomposite material used in e.g. aerospace application, involves oxidizing long-walled carbon nanotubes to obtain graphene nanobelt.
  • 专利号:   CN106566156-A, CN106566156-B
  • 发明人:   LI M, CHENG P, LUO G, XIONG Y, SHEN Q, ZHANG L
  • 专利权人:   UNIV WUHAN TECHNOLOGY
  • 国际专利分类:   C08J009/00, C08J009/12, C08K003/04, C08L033/12
  • 专利详细信息:   CN106566156-A 19 Apr 2017 C08L-033/12 201740 Pages: 13 Chinese
  • 申请详细信息:   CN106566156-A CN10943930 02 Nov 2016
  • 优先权号:   CN10943930

▎ 摘  要

NOVELTY - The preparation method of graphene nanobelt/poly(methyl methacrylate) micro-foamed nanocomposite material involves oxidizing long-walled carbon nanotubes to obtain graphene nanobelt, dispersing graphene nanobelt in dimethylformamide, and refluxing to obtain graphene nanobelt dispersion, blending dispersion with poly(methyl methacrylate), ultrasonically dispersing, anti-solvent precipitating, freeze-drying and hot-pressing to obtain graphene nanobelt/poly(methyl methacrylate) nanocomposite material, placing the nanocomposite material in a mold, and placing in a high pressure reactor. USE - Preparation of graphene nanobelt/poly(methyl methacrylate) micro-foamed nanocomposite material used in aerospace application, electronic packaging application, or automobile protection application. ADVANTAGE - The method enables the preparation of graphene nanobelt/poly(methyl methacrylate) micro-foamed nanocomposite material with small pore diameter, and high cell density, and mechanical strength. DETAILED DESCRIPTION - The preparation method of graphene nanobelt/poly(methyl methacrylate) micro-foamed nanocomposite material involves oxidizing long-walled carbon nanotubes to obtain graphene nanobelt, dispersing graphene nanobelt in dimethylformamide, and refluxing at high temperature to obtain graphene nanobelt dispersion, blending dispersion with poly(methyl methacrylate), ultrasonically dispersing, anti-solvent precipitating, freeze-drying and hot-pressing to obtain graphene nanobelt/poly(methyl methacrylate) nanocomposite material, placing the nanocomposite material in a mold, placing in a high pressure reactor, saturating with supercritical carbon dioxide, and rapidly decompressing.