• 专利标题:   Preparation of tantalum pentoxide nanoparticles/graphene composite photocatalyst for organic pollutant decomposition involves dissolving tantalum pentoxide precursor powder in hydrogen peroxide reagent to obtain tantalum peroxide precursor.
  • 专利号:   CN103084164-A, CN103084164-B
  • 发明人:   ZHANG D, MAO L, LU T, ZHU S, ZHU C
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   B01J023/20
  • 专利详细信息:   CN103084164-A 08 May 2013 B01J-023/20 201376 Pages: 8 Chinese
  • 申请详细信息:   CN103084164-A CN10044607 04 Feb 2013
  • 优先权号:   CN10044607

▎ 摘  要

NOVELTY - Tantalum pentoxide nanoparticles/graphene composite photocatalyst is prepared by dissolving tantalum pentoxide precursor powder in hydrogen peroxide reagent to obtain tantalum peroxide precursor solution, adding graphite oxide in precursor solution and performing ultrasonic dispersion, performing hydrothermal reaction, and centrifuging. USE - Preparation of tantalum pentoxide nanoparticles/graphene composite photocatalyst for organic pollutant decomposition. ADVANTAGE - Tantalum pentoxide nanoparticles/graphene composite photocatalyst has good conductivity and excellent performance and is environment-friendly. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of graphite oxide which involves adding concentrated sulfuric acid to sodium nitrate (NaNO3), flake graphite, and potassium permanganate under ice cooling, heating to 10-15 degrees C, stirring for 1 hour, heating to 35-40 degrees C for 1 hour, slowly adding de-ionized water and heating to 100 degrees C, adding 5 wt.% hydrogen peroxide solution dropwise, stirring for 1-2 hours, washing with 5 wt.% diluted hydrochloric acid solution, performing centrifugal filtration, and vacuum drying at 60-80 degrees C for 48 hours. DESCRIPTION OF DRAWING(S) - The drawing shows a scanning electron microscope image of tantalum pentoxide nanoparticles/graphene composite photocatalyst.