• 专利标题:   Preparation of graphene-polylactic acid antibacterial masterbatch for e.g. film, involves dissolving guanidine compound in water, adding obtained graphene oxide dispersion liquid, heating, freeze-drying, melt-mixing guanidine salt-graphene composite with polylactic acid, extruding, and granulating.
  • 专利号:   CN115322405-A
  • 发明人:   LIU H, BAI Y
  • 专利权人:   UNIV LANZHOU
  • 国际专利分类:   C08J003/22, C08K003/04, C08K005/31, C08K009/04, C08K009/12, C08L067/04
  • 专利详细信息:   CN115322405-A 11 Nov 2022 C08J-003/22 202305 Chinese
  • 申请详细信息:   CN115322405-A CN11052980 31 Aug 2022
  • 优先权号:   CN11052980

▎ 摘  要

NOVELTY - Preparation of graphene-polylactic acid antibacterial masterbatch involves (S1) using modified Hummers method to prepare uniformly dispersed graphene oxide dispersion liquid, (S2) dissolving guanidine compound in water, adding the obtained dispersion liquid, stirring and heating to make the guanidine compound molecule wound on the surface of graphene oxide two-dimensional sheet structure through electrostatic interaction, filtering, washing, and freeze-drying to obtain guanidine salt-graphene composite, and (S3) melt-mixing the guanidine salt-graphene composite with polylactic acid substrate, extruding, and granulating. USE - Preparation of graphene-polylactic acid antibacterial masterbatch used for preparing sheet material, film and nonwoven fabric (all claimed). ADVANTAGE - The masterbatch has excellent mechanical performance and antibacterial performance.